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GCMS analysis results for sample AE03246, March 2002

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03246 conducted on March 15, 2002.

NYC-WTC_000006105–000006125

Folder label: “GCMS X 2/12/02 A 3/01/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR01\03246.D Vial: 1 Acq On : 1 Mar 2002 4:00 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 14 Perylene-dl2 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 34.41 16.81 ug/L 11470700 Chrysene-dl2 30.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Perylene-dl2 264 C20D12 001520-96-3 96 2 Perylene-dl2 264 C20D12 001520-96-3 93 3 2-[N-(Diphenylmethylene)amino]-(... 263 C18H17DN2 000000-00-0 83 4 2-phenyl-3-(l-pyrrolin-2-yl)-5,6... 265 C17H19N3 102677-42-9 74 Abundance Scan 2749 (34.407 min): 03246. D (-) m/z 264.10 100.00% 264

5000 132 118 34.00 34.20 34.40 34.60 34.80 0- 52 64 76 88 102|| 156168180194,208220232 2521i 281 1 1 i 1 ■ m/z 263.10 41.01% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #190650: Perylene-d12 264

5000 34.00 34.20 34.40 34.60 34.80 m/z 132.00 26.07% 132 118 232 0A . | | t-'i 1 r"i‘']' i - । i11 । । । । I J n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #190649: Perylene-d12 264 ........ AY 1 i 1 1 34.00 34.20 34.40 34.60 34.80 5000 m/z 260.10 23.51% 132

118 232 0 1111,1 1 1 1,1 1 1 ' 1 ' 1 1 —IPTTTTTHm mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #203387:2-[N-(Diphenylmethylene)amino]-(2-2H)-3-methylbut... 264 34.00 34.20 34.40 34.60 34.80 m/z 130.00 21.59%

5000

0 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 34.00 34.20 34.40 34.60 34.80

03246.D HP022102.M Mon Mar 04 12:33:15 2002 Page 16

NYC-WTC_000006124

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NYC-WTC_000006124Source: NYC Law Department, mirrored locally

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