NYC 9/11 Public Portal Document
Cl- X Ca11 —Upull ICDOL
Data File : C:\MSDCHEM\l\5973N\02MAR01\0212B.D Vial: 1
Acq On : 1 Mar 2002 10:18 am Operator:
Sample : lab blank 2/12 Inst : Instrumen
Mise : March 1, 2002 Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator)
Title : 508 scan method
Library : C:\DATABASE\WILEY7N.L
********************************************* * * ********************* *
Peak Number 8 Cyclopentasiloxane, decamet... Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
12.54 0.43 ug/L 298655 Naphthalene-d8 13.20
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 68
2 3,4-Dihydroxybenzyl alcohol,tris... 356 C16H3203Si3 068595-79-9 49
3 N-(Trifluoroacetyl)-N,0,0',0''-t... 553 C22H42F3NO4Si4 000000-00-0 38
4 N-(Trifluoroacetyl)-0,0',O''-tri... 481 C19H34F3NO4Si3 000000-00-0 38
Abundance Scan 812 (12.540 min): 0212B.D (-) m/ z 73.00 100.00%
73
5000 267 355
45 12.20 12.40 12.60 12.80
125 154 191 237, 323 |
0/- — ■ i ' '' 1 ' i ■ ■ ' ■ i ■ ■ ■ 1 i 1 1 1 1 i 1 1 1 1 1 1 1 m/ z 266.90 44.98%
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #313068: Cyclopentasiloxane, decamethyl-
73
355
267 ........................ ..............................
5000
12.20 12.40 12.60 12.80
m/z 355.00 41.57%
207 323
0- PT—— +-=-+4 ' ' I । "i + I
n/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #302823: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)-
73
, ..... ,....
12.20 12.40 12.60 12.80
267 m/ z 356.00 16.02%
5000 179
356
n/z->
Abundance
0- 4445
50
147
11 1 1 1 1 1 1 1 1
100 150
209 237,
200 250
312 |
' ' ' i ' 1 ' ' i 1 ' ' ' I 1 1 1 1 I 1 1 1 1 1 1 ' 1 1 1 1 1
300 350 400 450 500 550 ........... ...........
#377151: N-(Trifluoroacetyl)-N,O,O',O“-tetrakis(trimethyl...
73 12.20 12.40 12.60 12.80
m/z 267.90 13.60%
355
5000
m/z->
45
0 1p
50 100
147
150
193 267
i lYrr । > -| i “i *
200 250
I 538
■ i 1 1 1 ' i 1 ■ ' ' i 1 ' 1 1 I ' 1 1 1 I ' 1 1 '' I 1 '
300 350 400 450 500 550
.mm
12.20 12.40 12.60 12.80
212B.D HP022102.M Mon Mar 04 12:32:45 2002 Page 10
NYC-WTC_000006038
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