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GCMS surrogate recovery results, sample AE03018, March 2002

Machine-extracted title · confidence 95%

Analytical report showing surrogate recovery data for sample AE03018 analyzed on March 12, 2002.

NYC-WTC_000005916–000005924

Folder label: “GCMS X 2/12/02 A 2/28/02

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Scanned page image, NYC-WTC_000005921
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\MSDCHEM\1\DATA\022802\03017.D Vial: 10 Acq On 1 Mar 2002 7:45 pm Operator: McLean Sample 2/12/02 GC SCAN Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.598 275 278 293 rBV 132547 436594 4.77% 0.868% 2 9.570 711 716 736 rBV 2514592 6282814 68.64% 12.493% 3 13.053 1094 1100 1114 rBV 4577301 8527162 93.16% 16.955% 4 18.160 1657 1663 1679 rBV 4373157 9043601 98.80% 17.982% 5 22.523 2138 2144 2158 rBV2 4268783 9153052 100.00% 18.200%

6 27.457 2683 2688 2698 rBV 635532 1164548 12.72% 2.316% 7 30.341 2998 3006 3022 rBV 3729433 9027636 98.63% 17.950% 8 34.214 3425 3433 3451 rBV 2698564 6656750 72.73% 13.236%

Sum of corrected areas: 50292157

)3017.D 5080202.M Mon Mar 04 05:42:01 2002 Page 1

NYC-WTC_000005921

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NYC-WTC_000005921Source: NYC Law Department, mirrored locally

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