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GCMS surrogate recovery results for sample AE03021, March 2002

Machine-extracted title · confidence 90%

Analytical report showing surrogate recovery data for sample AE03021 analyzed on March 12, 2002.

NYC-WTC_000005955–000005962

Folder label: “GCMS X 2/12/02 A 2/28/02

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Scanned page image, NYC-WTC_000005960
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NYC 9/11 Public Portal Document LSC Area Percent Report

■Data File C:\MSDCHEM\l\DATA\022802\03071.D Vial: 15 Acq On 1 Mar 2002 11:49 pm Operator: McLean Sample 2/12/02 GC SCAN Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.597 275 278 293 rBV 104938 351989 4.02% 0.733% 2 9.570 711 716 734 rBV 2290947 5941756 67.78% 12.375% 3 13.053 1094 1100 1116 rBV 4292802 8042911 91.75% 16.751% 4 18.160 1657 1663 1677 rBV 4340393 8542497 97.45% 17.791% 5 22.523 2138 2144 2158 rBV2 4047771 8676162 98.98% 18.070%

6 27.457 2683 2688 2699 rBB 628315 1127450 12.86% 2.348% 7 30.332 2998 3005 3024 rBV2 3619827 8765997 100.00% 18.257% 8 34.214 3425 3433 3450 rBV 2754080 6566608 74.91% 13.676%

Sum of corrected areas: 48015370

071.D 5080202.M Mon Mar 04 05:46:17 2002 Page 1

NYC-WTC_000005960

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NYC-WTC_000005960Source: NYC Law Department, mirrored locally

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