GCMS analysis results for sample AE03073, March 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\MSDCHEM\1\DATA\022802\03073.D Vial: 7 Acq On 1 Mar 2002 5:18 pm Operator: McLean Sample 2/12/02 GC SCAN Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total' 1 3.865 84 87 94 rBV 69793 143599 1.50% 0.274% 2 5.597 275 278 294 rBV 158940 483989 5.06% 0.924% 3 9.579 712 717 732 rBV 2653563 6439626 67.29% 12.291% 4 13.053 1094 1100 1115 rBV 4711812 8758534 91.53% 16.717% 5 18.169 1657 1664 1684 rBV 4559262 9374099 97.96% 17.892% 6 22.522 2137 2144 2156 rBV2 4339179 9504079 99.32% 18.140% 7 27.457 2683 2688 2698 rBV 719040 1277000 13.34% 2.437% 8 30.341 2998 3006 3026 rBV2 3989364 9569319 100.00% 18.265% 9 34.214 3425 3433 3444 rBV 2759157 6842453 71.50% 13.060%

Sum of corrected areas: 52392698

J073.D 5080202.M Mon Mar 04 05:51:35 2002 Page 1

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