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GCMS surrogate recovery results for sample AE03072, March 2002

Machine-extracted title · confidence 100%

Analytical report showing surrogate recovery data for sample AE03072 analyzed on March 12, 2002.

NYC-WTC_000005963–000005972

Folder label: “GCMS X 2/12/02 A 2/28/02

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Scanned page image, NYC-WTC_000005968
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\MSDCHEM\1\DATA\022802\03072.D Vial: 6 . Acq On 1 Mar 2002 4:29 pm Operator: McLean Sample 2/12/02 GC SCAN Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.865 84 87 93 rBV2 66740 142212 1.51% 0.277% 2 5.597 275 278 289 rBV 134128 397878 4.23% 0.774% 3 9.579 711 717 746 rBV 2618330 6471660 68.88% 12.585% 4 13.053 1094 1100 1116 rBV 4639436 8686287 92.45% 16.892% 5 18.169 1657 1664 1680 rBV 4521680 9261187 98.57% 18.010%

6 22.522 2138 2144 2158 rBV2 4341012 9395858 100.00% 18.271% 7 27.457 2683 2688 2698 rVB 697904 1273339 13.55% 2.476% 8 30.341 2998 3006 3022 rBV2 3827573 9175654 97.66% 17.843% 9 34.214 3425 3433 3451 rBV2 2661258 6619800 70.45% 12.873%

Sum of corrected areas: 51423875

13072.D 5080202.M Mon Mar 04 05:50:11 2002 Page 1

NYC-WTC_000005968

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NYC-WTC_000005968Source: NYC Law Department, mirrored locally

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