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GCMS analysis results for sample AD31662, Feb 2002

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Gas chromatography-mass spectrometry analysis of environmental sample AD31662 conducted on February 15, 2002.

NYC-WTC_000005747–000005750

Folder label: “GCMS X 2/11/02 A 2/13/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\FEB1102\CAL8 OB.D Vial: 2 Acq On 13 Feb 2002 9:51 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 15 9:45 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.39 168 1839794 85.08 ug/1 # 91 31) 4-Bromophenyl-phenylether 24.43 248 1177678 84.26 ug/1 98 32) Hexachlorobenzene 24.88 284 1354013 82.71 ug/1 97 33) Phenanthrene 25.87 178 5784107 86.71 ug/1 100 3 4) Anthracene 26.00 178 5605894 85.78 ug/1 100 35) Di-n-butylphthalate 27.75 149 8144815 87.37 ug/1 99 36) Fluoranthene 29.50 202 6105997 91.69 ug/1 96 3 9) Pyrene 30.18 202 6262272 80.00 ug/1 94 40) Butylbenzylphthalate 32.28 149 3386733 78.14 ug/1 99 41) Benzo(a)anthracene 33.82 228 4955302 86.58 ug/1 99 42) Bis(2-ethylhexyl)phthalate 34.05 149 4391835 75.02 ug/1 99 43) Chrysene 33.95 228 4753233 84.40 ug/1 99 45) Di-n-Octylphthalate 35.80 149 6826450 77.98 ug/1 # 98 46) Benzo(b)fluoranthene 36.96 252 4545874 92.02 ug/1 99 47) Benzo(k)fluoranthene 37.04 252 4378657m 88.20 ug/1 48) Benzo(a)pyrene 37.98 252 3608539 88.12 ug/1 98 49) Indeno(1,2,3-cd)pyrene 42.45 276 3641778 97.45 uq/1 98 50) Dibenz(a,h)anthracene 42.53 278 2926502m( 102.47 ug/1 51) Benzo(g,h,i)perylene 43.76 276 2797403 92.85 ug/l 99

(#) = qualifier out of range (m) = manual integration CAL80B.D GCMS0208.M Fri Feb 15 09:45:42 2002 Page 2

NYC-WTC_000005749

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NYC-WTC_000005749Source: NYC Law Department, mirrored locally

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