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GCMS analysis results for sample AD31344, Feb 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis of environmental sample AD31344 conducted on February 15, 2002.

NYC-WTC_000005707–000005715

Folder label: “GCMS X 2/7/02 A 2/9/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\FEB0802\31344.D Vial: 40 Acq On 9 Feb 2002 11:11 pm Operator: 209 GALOS Sample RE-EXTRACT 2/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.217 342 346 361 rBV 104559 312788 8.37% 1.619% 2 12.348 790 796 809 rVB 1160240 2780181 74.39% 14.392% 3 15.993 1186 1193 1209 rBV 1764078 3481770 93.16% 18.024% 4 21.308 1765 1772 1786 rBV 1888009 3737265 100.00% 19.347% 5 25.760 2249 2257 2267 rBV 1693454 3642201 97.46% 18.855%

6 30.828 2804 2809 2814 rBV 205328 384348 10.28% 1.990% 7 33.821 3128 3135 3150 rBV2 1185546 2814012 75.30% 14.567% 8 38.117 3593 3603 3620 rBV 699457 2164593 57.92% 11.206%

Sum of corrected areas: 19317158

31344.D GCMS0208.M Wed Feb 13 11:15:11 2002

NYC-WTC_000005712

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NYC-WTC_000005712Source: NYC Law Department, mirrored locally

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