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GCMS analysis results for sample AD31341 with surrogate data, Feb

Machine-extracted title · confidence 50%

Laboratory report for sample AD31341 showing GCMS analysis of unknown compounds and surrogate recovery on February 15, 2002.

NYC-WTC_000003880–000003890

Folder label: “GCMS X 1/28/02 A 2/8/02

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Scanned page image, NYC-WTC_000003885
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\FEB0802\31341.D Vial: 25 Acq On 9 Feb 2002 8:39 am Operator: 209 GALOS Sample RE-EXTRACT 1/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.050 759 763 770 rVB 12252 28993 1.14% 0.229% 2 12.271 783 787 790 rBV 18626 41434 1.63% 0.327% 3 12.344 790 795 809 rVB 820688 1947965 76.80% 15.354% 4 15.989 1186 1192 1210 rBV 1223822 2389693 94.22% 18.835% 5 21.304 1765 1771 1783 rBV 1251879 2536295 100.00% 19.991%

6 25.756 2249 2256 2267 rBV 1180899 2458988 96.95% 19.382% 7 27.712 2462 2469 2477 rBV 14772 26629 1.05% 0.210% 8 30.833 2804 2809 2815 rVB 115634 215139 8.48% 1.696% 9 33.826 3128 3135 3154 rBV 784939 1759733 69.38% 13.870% 10 38.104 3593 3601 3618 rBV2 430830 1282423 50.56% 10.108%

Sum of corrected areas: 12687292

31341.D GCMS0208.M Thu Feb 14 15:03:03 2002

NYC-WTC_000003885

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NYC-WTC_000003885Source: NYC Law Department, mirrored locally

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