NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\FEB 0802\LBB.D Vial: 28
Acq On 9 Feb 2002 11:34 am Operator: 209 GALOS
Sample GC/MS SCAN 2/7 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Feb 13 9:42 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Fri Feb 08 15:29:22 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.35 152 345307 20.00 ug/1 0.00
10) Naphthalene-d8 15.99 136 1333661 20.00 ug/1 0.00
17) Acenaphthene-diO 21.30 164 710567 20.00 ug/1 0.00
29) Phenanthrene-diO 25.76 188 1017235 20.00 ug/1 0.00
38) Chrysene-dl2 33.83 240 682012 20.00 ug/1 -0.02
44) Perylene-dl2 38.11 264 472978 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.83 235 46537 3.68 ug/mL 0.34
Spiked Amount 5.000 Recovery = 73.60%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 11.75 93 547 N.D.
4) 1,3-Dichlorobenzene 12.24 146 656 N.D.
5) 1,4-Dichlorobenzene 12.40 146 744 N.D.
6) 1,2-Dichlorobenzene 12.91 146 666 N.D.
7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 14.03 77 489 N.D.
12) Isophorone 14.69 82 873 N.D.
13) bis(2-Chloroethoxy)methane 15.36 93 691 N.D.
14) 1,2,4-Trichlorobenzene 15.88 180 556 N.D.
15) Naphthalene 16.04 128 2640 N.D.
16) Hexachlorobutadiene 16.59 225 100 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 19.55 162 1137 N.D.
20) Dimethylphthalate 20.64 163 1309 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
2 2) Acenaphthylene 20.84 152 1415 N.D.
23) Acenaphthene 21.40 153 1334 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.78 149 1276 N.D.
26) 4-Chlorophenyl-phenylether 22.94 204 494 N.D.
27) Fluorene 22.91 166 1248 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
LBB.D GCMS0208.M Wed Feb 13 09:43:30 2002 Page 1
NYC-WTC_000005620
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