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GCMS blank analysis results for sample AE02966, February 2002

Machine-extracted title · confidence 100%

Blank analysis report for DEP sample AE02966 showing all target compounds below minimum detection limits.

NYC-WTC_000005619–000005626

Folder label: “GCMS X 2/7/02 A 2/9/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\FEB 0802\LBB.D Vial: 28 Acq On 9 Feb 2002 11:34 am Operator: 209 GALOS Sample GC/MS SCAN 2/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 13 9:42 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Feb 08 15:29:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.35 152 345307 20.00 ug/1 0.00 10) Naphthalene-d8 15.99 136 1333661 20.00 ug/1 0.00 17) Acenaphthene-diO 21.30 164 710567 20.00 ug/1 0.00 29) Phenanthrene-diO 25.76 188 1017235 20.00 ug/1 0.00 38) Chrysene-dl2 33.83 240 682012 20.00 ug/1 -0.02 44) Perylene-dl2 38.11 264 472978 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.83 235 46537 3.68 ug/mL 0.34 Spiked Amount 5.000 Recovery = 73.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 11.75 93 547 N.D. 4) 1,3-Dichlorobenzene 12.24 146 656 N.D. 5) 1,4-Dichlorobenzene 12.40 146 744 N.D. 6) 1,2-Dichlorobenzene 12.91 146 666 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 14.03 77 489 N.D. 12) Isophorone 14.69 82 873 N.D. 13) bis(2-Chloroethoxy)methane 15.36 93 691 N.D. 14) 1,2,4-Trichlorobenzene 15.88 180 556 N.D. 15) Naphthalene 16.04 128 2640 N.D. 16) Hexachlorobutadiene 16.59 225 100 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 19.55 162 1137 N.D. 20) Dimethylphthalate 20.64 163 1309 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 20.84 152 1415 N.D. 23) Acenaphthene 21.40 153 1334 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.78 149 1276 N.D. 26) 4-Chlorophenyl-phenylether 22.94 204 494 N.D. 27) Fluorene 22.91 166 1248 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration LBB.D GCMS0208.M Wed Feb 13 09:43:30 2002 Page 1

NYC-WTC_000005620

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NYC-WTC_000005620Source: NYC Law Department, mirrored locally

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