Blank sample analysis report confirming no contamination above method detection limits for target compounds analyzed on February 1, 2002.
NYC-WTC_000005159–000005166Folder label: “GCMS X 2/4/02 A 2/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\FEB 0 8 0 2\LB.D Vial: 5 Acq On 8 Feb 2002 1:11 pm Operator: 209 GALOS Sample GC/MS SCAN 2/8 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 11 12:00 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Feb 08 15:29:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.35 152 303271 20.00 ug/1 0.00 10) Naphthalene-d8 15.99 136 1146968 20.00 ug/1 0.00 17) Acenaphthene-diO 21.31 164 606193 20.00 ug/1 0.00 29) Phenanthrene-diO 25.76 188 864512 20.00 ug/1 0.00 38) Chrysene-dl2 33.83 240 575726 20.00 ug/1 -0.02 44) Perylene-dl2 38.12 264 364747 20.00 ug/1 0.00
System Monitoring Compounds 37) 2,4-DDD 30.84 235 49587 4.61 ug/mL 0.34 Spiked Amount 5.000 Recovery = 92.20%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 11.59 93 188 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2‘-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration LB.D GCMS0208.M Mon Feb 11 12:01:30 2002 Page 1
NYC-WTC_000005160
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