GCMS analysis results for sample AE00845, Feb 2002

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Laboratory report documenting GCMS analysis of sample AE00845 conducted on February 11, 2002, including surrogate recovery data.

NYC-WTC_000005202–000005209

Folder label: “GCMS X 2/4/02 A 2/8/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C: \HPCHEM\1\DATA\FEB0802\00845.D Vial: 11 Acq On 8 Feb 2002 7:04 pm Operator: 209 GALOS Sample GC/MS SCAN 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 11 12:13 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Feb 08 15:29:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.35 152 297571 20.00 ug/1 0.00 10) Naphthalene-d8 15.99 136 1131533 20.00 ug/1 0.00 17) Acenaphthene-diO 21.31 164 598296 20.00 ug/1 0.00 29) Phenanthrene-diO 25.75 188 854893 20.00 ug/1 -0.01 38) Chrysene-dl2 33.82 240 561177 20.00 ug/1 -0.02 44) Perylene-dl2 38.11 264 366846 20.00 ug/1 -0.01

System Monitoring Compounds 37) 2,4-DDD 30.84 235 44451 4.18 ug/mL 0.34 Spiked Amount 5.000 Recovery = 83.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.79 149 246 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 00845.D GCMS0208.M Mon Feb 11 12:13:56 2002 Page 1

NYC-WTC_000005204

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GCMS analysis results, sample AE00831, February 2002 · Box DEP Box 12

NYC-WTC_000005194

Gas chromatography-mass spectrometry analysis of sample AE00831 performed on 2/11/02, detecting unknown compounds and 2,4-DDD surrogate at 81 ug.

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