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GCMS analysis results for sample AE02712, Mar 15, 2002

Machine-extracted title · confidence 90%

Laboratory report listing unknown compounds and surrogate recovery data for sample AE02712.

NYC-WTC_000005484–000005494

Folder label: “GCMS X 2/5/02 A 3/7/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR0702\2712.D Vial: 23 Acq On 8 Mar 2002 11:22 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.83 0.20 ug/1 31924 Phenanthrene-dl0 25.69

Hit# of 5 Tentative / / ID MW MolForm CAS# Qual

1 Anthracene-d10-/y 7 188 C14D10 001719-06-8 90 2 Phenanthrene-410/ 188 C14D10 001517-22-2 90 3 Pyrrolo[2,3-b]indole, 1,2,3,3a,8,8a 188 C12H16N2 004089-16-1 42 4 4-Fluoro-6ymethyl-2-phenylpyrimidin 188 C11H9FN2 000000-00-0 42 Abundance 7 Scan 2264 (25.829 min): 2712.D (-) m/ z 188.10 100.00% 188

5000

80 94 160 25.40 25.60 25.80 26.00 26.20

m/z-> 1.86 60 ... 801. ----- 70 | 90 100 110 120 130 140 150 160 170 180 190 T m/z 18 9.10 14.04%! Abundance #19957: Anthracene-d'O- 188 ......... ..... ......................... 5000 25.40 25.60 25.80 26.00 26.20 m/ z 8 .10 13.61% 66 80 94 J60 4 1—0. /000 T/?-? 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 138

25.40 25.60 25.80 26.00 26.20 5000 m/z 184.10 12.36%

80 94 160 66 m/z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 .................................................... Abundance #19922: Pyrrolo[2,3-b]indoie. 1,2,3,3a.8.8a-hexahydro-3a.8- 144 Us 25.40 25.60 25.80 26.00 26.20 158 m/z 94.00 10.77% 5000

173 - m/z-> ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ t ■ ■ ■ ■ । ■ ■ ■ ■ । ■ > < ■ । 60 70 80 90 100 110 120 130 140 150 ■ TT 160 170 180 I190— ......... ......................... 25.40 25.60 25.80 26.00 26.20 |

2712.D GCMS0208.M Wed Mar 13 15:01:45 2002 Page 3

NYC-WTC_000005493

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NYC-WTC_000005493Source: NYC Law Department, mirrored locally

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