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GCMS analysis results for sample AE02600, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02600 conducted on March 7, 2002, including surrogate recovery data.

NYC-WTC_000005312–000005321

Folder label: “GCMS X 2/5/02 A 3/1/02

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Scanned page image, NYC-WTC_000005317
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Keport

Data File C:\HPCHEM\l\DATA\MAR0102\2600.D Vial: 10 Acq On 1 Mar 2002 5:13 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.195 339 343 353 rBV 11840 28318 1.20% 0.235% 2 12.317 786 792 810 rVB 688194 1638118 69.16% 13.570% 3 15.953 1182 1188 1207 rBV 986744 2176413 91.88% 18.029% 4 21.268 1761 1767 1789 rBV 1068926 2368628 100.00% 19.621% 5 25.711 2245 2251 2264 rBV2 954185 2268122 95.76% 18.788%

6 25.858 2264 2267 2283 rVB 10146 31861 1.35% 0.264% 7 30.788 2799 2804 2813 rBV 138221 294057 12.41% 2.436% 8 33.781 3123 3130 3148 rBV2 766911 1821639 76.91% 15.090% 9 38.059 3587 3596 3614 rBV2 444497 1444788 61.00% 11.968%

Sum of corrected areas: 12071944

2600.D GCMS0208.M Mon Mar 04 11:44:08 2002

NYC-WTC_000005317

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NYC-WTC_000005317Source: NYC Law Department, mirrored locally

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