GCMS method 508 scan data, March 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\MAR3002\4849.D Vial: 6 Acq On : 29 Mar 2002 7:55 pm Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2- Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.137 333 337 345 rBV 16123 38636 1.05% 0.221% 2 12.250 779 785 803 rVB 1050583 2521812 68.28% 14.394% 3 14.848 1062 1068 1074 rVB 22076 40389 1.09% 0.231% 4 15.885 1175 1181 1194 rBV 1596736 3261224 88.30% 18.614% 5 21.191 1753 1759 1780 rBV 1775242 3693147 100.00% 21.080%

6 25.635 2236 2243 2254 rBV 1677011 3450493 93.43% 19.695% 7 30.711 2790 2796 2801 rBV 212234 420611 11.39% 2.401% 8 33.328 3075 3081 3097^rBV 280859 607030 16.44% 3.465% 9 33.695 3109 3121 3139 rBV 921672 2105823 57.02% 12.020% 10 37.936 3574 3583 3603 rBV2 456498 1380809 37.39% 7.881%

Sum of corrected areas: 17519974

4849.D GCMS0308.M Tue Apr 02 11:03:17 2002

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