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GCMS analysis results for sample AE02595, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02595 conducted on March 7, 2002, including surrogate recovery data.

NYC-WTC_000005261–000005270

Folder label: “GCMS X 2/5/02 A 3/1/02

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Scanned page image, NYC-WTC_000005268
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NYC 9/11 Public Portal Document ulbrary bearcn compourd KCpOLL

Data File : C:\HPCHEM\l\DATA\MAR0102\2595.D Vial: 5 Acq On : 1 Mar 2002 12:17 pm Operator: Sample : gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Benzenesulfonic acid, 4-methox Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.23 ug/1 23842 Phenanthrene-dl0 25.72

Hit# of 2 Tentative ID MW MolForm CAS# Qual

1 Benzenesulfonic acid, 4-methoxy- 188 C7H804S 005857-42-1 3 2 Bisethoxo (methoxo) oxovanadium 188 C5H13O4V 062450-00-4 1

Abundance Scan 2267 (25.855 min): 2595.D (-) m/ z 188.10 100.00% 188

8000

6000 ,................................. 4000 25.60 25.80 26.00 26.20 m/z 94.00 17.91% 2000 94 40 156 1 66 11 " ' • i " " I'1'' i " " i' " ' i1 l ■ ■1 140 ■ i - 90 100 110 120 130 150 160 170 180 190 " ’ m/z--> 20 30 40 50 60 70 80 Abundance #19714: Benzenesulfonic acid, 4-methoxy- ...... ........................ 188 > ■ i । । । । I ' , i , । । । । , _______ 25.60 25.80 26.00 26.20 8000 1 m/z 78.05 11.98% 123 6000

4000- 77 .............................. ................... 92 107 2000 64 171 25.60 25.80 26.00 26.20 I 155 I m/z 39.95 9.96% ‘I‘‘‘‘1‘4‘‘1‘*1‘I/‘A+11+*41‘/"411 TCuIII0000177nfi ■' i'' " i " '' i " " i " II’ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 31

8000 ........... .

25.60 25.80 26.00 26.20 6000- 110 m/z 155.85 9.91% 45 4000

173 187 2000- 155 141 127 TTTTTTTTTTTLUTTTTTTTTTTTTTTTTTTTTTTTTTTTLTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTITTTTTT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

2595.D GCMS0208.M Mon Mar 04 11:39:30 2002 Page 1

NYC-WTC_000005268

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NYC-WTC_000005268Source: NYC Law Department, mirrored locally

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