DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\0201B.D Vial: 1 Acq On : 27 Feb 2002 10:33 am Operator: Sample : lab blank 2/1 Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 12 Pyrene (CAS) $$ .beta.-Pyre... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

26.22 0.03 ug/L 21194 Phenanthrene-dl0 22.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyrene (CAS) $$ .beta.-Pyrene $$... 202 C16H10 000129-00-0 64 2 Pyrene $$ .beta.-Pyrene $$ Benzo... 202 C16H10 000129-00-0 64 3 Pyrene 202 C16H10 000129-00-0 59 4 Fluoranthene 202 C16H10 000206-44-0 59 Abundance Scan 2024 (26.222 min): 0201 B.D (-) m/z 202.00 100.00% 202

5000

49 100 25.80 26.00 26.20 26.40 26.60

n/z-> 0 .... .............. ‘11 ‘1 11 11 ‘ ‘11 11 1 ‘ I'' 1111' 11 1 ■1 M 1. 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/ Z 2 00.00 19.83%

Abundance #118630: Pyrene (CAS) $$ .beta.-Pyrene $$ Benzo[def]phenan... 202

5000 i ■ ■ ■ ■ । 1 1 111‘+I‘ 101 25.80 26.00 26.20 26.40 26.60 m/z 99.90 16.00% 150 174 J ol ‘1′1′11′1′414 111'1 ■ ■ I " 1 ■ i11 ■ ■ i ■ " 'T' " ■ i1111111,1111" 11 ■ " "i ur m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #118626: Pyrene $$ beta.-Pyrene $$ Benzo[def]phenanthrene... 2012 i ■ 1 ■ ■ । ‘ ■ 1 ■ i ■ ■ ■ ■ । '

25.80 26.00 26.20 26.40 26.60 5000 m/z 203.10 14.33%

— 101 ,1 88 ,1 150 163 174 | 0 " i" " i" " i" " i"111111,111" 'T111111'1111111111111"11P1111111' i1''' 1111111111 I’I’ TII’ n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #118629: Pyrene i ■ ■ ■ r i ' ' ■ 1 । ■ 1 1 । ■ 202 25.80 26.00 26.20 26.40 26.60 m/z 101.00 12.87%

5000 101 88 150 174 | 0 11 ■' i " " i " 1' i " " i " 111........ 111' 111 i'i 1111 > 11 ■ 111′1′1 TT-fT "TI ■ ‘ । 1 1 1 ’ । ‘ n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 25.80 26.00 26.20 26.40 26.60

201B.D HP022102.M Thu Feb 28 08:46:41 2002 Page 14

NYC-WTC_000004962

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NYC-WTC_000004962Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999