DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30703.D Vial: 43 Acq On : 30 Dec 2001 12:31 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.72 2.38 ug/1 1127710 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, A-hydroxy-4-methyl- 116 C6H1202 000123-42-2 56 2 3-Hydroxy-2 -pentanone 102 C5H10O2 003142-66-3 9 3 Propanenitrile, 3-ethoxy- 99 C5H9NO 002141-62-0 9 4 Morpholine/ 4-methyl-________________ 101 C5H11NO 000109-02-4 9 Abundance Scan 291 (7.718 min): 30703.D (-) m/ z42.95 100.00% 43

5000 59

101 ' 1 ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' 1 I | 67 75 83 88 , | 7.40 7.60 7.80 8.00 m/z-> 110 ..... 20 30 38,140 50 53 , I | ' । 1 1 I । ' 1 ' I ।'' 1 1 I ' ‘ 1 I । । 60 70 80 90 100 । । . 110 m/ z 59.0,5 48.87% Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

/, ■ 1 । । । 5000 59 7.40 7.60 7.80 8.00 m/z 101.05 19.23% 27 101

m/z-> ------- 10 20 30 40 +49+ 50 83 —Iumm—muuBOTIT 60 70 80 90 100 | 110 Abundance 41691: 3-Hydroxy-2-pentarone 31 59 1 1 1 I 1 1 ' 1 I ' ‘ ' 11Tm- 1 1 1 I I 7.40 7.60 7.80 8.00 5000 m/z 58.05 15.50% 45 15 i 66 73 84 102 ' ' I ‘ ' I ' 1 ' ' I ‘ 1 ' ' I ' ' ' I ' ‘ ‘ ' I ’ 1 ‘ ' I ' ' 1 ' 1 ' ‘ 1 ’ I ' 1 ' ' I 1 ' ' ' I ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63285: Propanenitrile, 3-ethoxy- — ——— 31 7.40 7.60 7.80 8.00 m/ z 41. 05 7.59% 54 5000 59

2C 45

m/z-> ■ ■ i 10 ' ■ 1 ■ i 20 -4430 00 40 50 1 1 1 1 ' 60 70 ■ i ■ ■ ■ ■ i ■

80 841 ■ ■ i ’ ' ' 981 i ■ ' ' 1 I 1 90 100 110 7.40 7.60 7.80 8.00

30703.D GCMS1126.M Mon Jan 28 11:20:24 2002 Page 2

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