NYC-WTC_000003639
Laboratory report documenting GCMS analysis of sample AE01499 conducted on March 6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Document / 7 pages
DEP GCMS unknown compounds report, Mar 2002
Machine-extracted title · confidence 95%GCMS analysis report dated March 6, 2002, listing other unknown compounds and surrogate recovery data for a different sample.
NYC-WTC_000003729–000003735Folder label: “GCMS X 1/25/02 A 2/26/02”
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vial ’• 4 X -X 35 .D operato: ( Nve or Public Porta bocumen Quantitation Report (QT Reviewed)
EM\1\DATA\FEB2502\1735.D Vial: 21 D o 2002 7:12 am Operator: s scan 1/25 fb Inst : GC/MS 209 s 9 On Multiplr: 1.00 M""Ple_on Params: GOOFY. P Ms - Feb 28 11:27 2002 Quant Results File: GCMS0208.RE Qu > Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Qw : 209 625/TCLP calibration table Jt Update : Wed Feb 27 11:30:15 2002 esponse via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.31 152 239552 20.00 ug/1 -0.04 10) Naphthalene-d8 15.96 136 906265 20.00 ug/1 -0.04 17) Acenaphthene-diO 21.27 164 483379 20.00 ug/1 -0.05 29) Phenanthrene-diO 25.72 188 671322 20.00 ug/1 -0.05 38) Chrysene-dl2 33.78 240 446996 20.00 ug/1 -0.07 44) Perylene-dl2 38.05 264 303614 20.00 ug/1 -0.08
System Monitoring Compounds 37) 2,4-DDD 30.79 235 37179 5.30 ug/mL 0.30 Spiked Amount 5.000 Recovery = 106.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis (2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Is opho rone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.01 128 193 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 10) Dimethylphthalate 0.00 163 0 N.D. 1) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2) Acenaphthylene 0.00 152 0 N.D. 3) Acenaphthene 0.00 153 0 N.D. 1) 2,4-Dinitrotoluene 0.00 165 0 N.D. i) Diethylphthalate 0.00 149 0 N.D. ) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. ) Fluorene 0.00 166 0 N.D. ' Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
= qualifier out of range (m) = manual integration .D GCMS0208.M Thu Feb 28 11:28:03 2002
NYC-WTC_000003731
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NYC-WTC_000003731Source: NYC Law Department, mirrored locally
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