GCMS analysis results for sample AE01140, Feb 2002

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Laboratory report documenting GCMS analysis of sample AE01140 conducted on February 27, 2002.

NYC-WTC_000003503–000003522

Folder label: “GCMS X 1/20/02 A 2/25/02”

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NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02FEB25\01140.D Vial: 6 Acq' On : 25 Feb 2002 3 :22 pm Operator: • ' Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 6 1,3,5-Cycloheptatriene Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

4.38 0.07 ug/L 25360 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 39 2 METHYLFULVENE 92 C7H8 000000-00-0 9 3 1,3,5-Cycloheptatriene (CAS) $$ ... 92 C7H8 000544-25-2 9 4 1,3,5-Cycloheptatriene $$ Cycloh... 92 C7H8 000544-25-2 7 Abundance Scan 89 (4.378 min): 01140.D (-) m/ z 91.00 100.00% 91

5000

i ■ ■ • ■ । - i ■

43 51 65 84 4.00 4.20 4.40 4.60 4.80 O+ ----- m/ z 92.00 65.91% J ■ > i ■ ■ ■ ■ i ■ ■

m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5569:1,3,5-Cycloheptatriene 91

— 5000 ‘ i ■ ■ ■ ■ i ' 4.00 4.20 4.40 4.60 4.80 65 m/z 65.00 10.61% 27 37 46 51 61,| Ot " I " " 111" I " " I'1" I " " 11 " ' 11' ........... ....1111111 ■ i ■ ■ ■ ■ । ■ ■ ■ • । ■ ■ ■ ■ । ■ i | 11 r^'rrT miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5531: METHYLFULVENE 91 4.00 4.20 4.40 4.60 4.80 5000 m/ z 50.90 9.62% N 39 65 I 45 61 , I, Of 1 FPri 1 fr! I I | I I ! I | I 1 I I | ,,,, | I I I I | I ! I . | I I I I | I I I I | I I H | I I !> | I I ! I | I 1 I I | ! !! t [ I I 1111" 1111 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5568:1,3,5-Cycloheptatriene (CAS) $$ Cycloheptatriene $$... 91 4.00 4.20 4.40 4.60 4.80 m/z 43.10 8.66%

5000

39 61 65 1 1 I " " I " " I 1 ' ' ' I HPn I I I I | I I ! I | I I ! 1 | I I I I | I I 1 86 0 ! T .-n-j- . ........... IT’ ■ ■ ■ ] | < < ■ I ■ | m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 4.00 4.20 4.40 4.60 4.80

01140.D HP022102.M Tue Feb 26 08:30:17 2002 Page 8

NYC-WTC_000003514

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GCMS analysis results, sample AE01139, 2,4-DDD, Feb 2002 · Box DEP Box 12

NYC-WTC_000003483

Gas chromatography-mass spectrometry analysis report for sample AE01139 detecting surrogate 2,4-DDD at 76 ug with MDL of 5.0, analyzed on 02/27/2002.

1 shared topics · Same agency, volume and box · similarity 0.998