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VOCs GC/MS analysis results, Jan 22-23 2002

Machine-extracted title · confidence 90%

Laboratory report showing volatile organic compound analysis results for sample AE01036 processed on January 22 and 23, 2002.

NYC-WTC_000003249–000003325

Folder label: “524 1/22/02”

Page image
Scanned page image, NYC-WTC_000003286
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02JAN22\00917.D Vial: 12 Acq On : 22 Jan 2002 6:34 pm Operator: Sample : nyc Inst : 210 Misc : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP010802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Cyclotetrasiloxane, octamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 26.63 0.04 ug/L 16452 CHLOROBENZENE-D5 25.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 72 2 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 5 3 Morphinan, 7,8-didehydro-3-methoxy- 281 C19H23NO 001816-06-4 5 d 9 7_Rrmn,7n-r~HonrNtH .7 ,T c_G G_r7ir,vir7c 0P1 (1 1 11TT(17C nnnnnn_nn_n Z

Abundance Scan 2033 (26.633 min): 00917.D (-) m Z 280. 95 100. 00% 21

5000

44 91 106 133 73 191 207 26.2p 26.40 26.60 26.80 27.00 m z 281.95 32.01% /z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 undance #72646: Cyclotetrasiloxane, octamethyl. 21

5000 26.2p 26.40 26.60 26.80 27.00 m z 282.95 23.81% 73 265 45 59 133 1n 193 207 235 z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 undance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 21

26.2c 26.40 26.60 26.80 27.00 5000 m Z Y6

253 126 203 266 224 240 z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 undance #39628: Morphinan, 7,8-didehydro-3-methoxy-17-methyl-6-meth 2I 26.20 26.40 26.60 26.80 27.00 m z 44.05 15.29%

5000 44 160 147 188 226 266 208 i i 238 i i /z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 26.20 26.40 26.60 26.80 27.00

00917.D HP010802.M Wed Jan 23 09:42:06 2002 Page 5

NYC-WTC 000003286

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NYC-WTC_000003286Source: NYC Law Department, mirrored locally

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