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VOCs GC/MS analysis results, Jan 22-23 2002

Machine-extracted title · confidence 90%

Laboratory report showing volatile organic compound analysis results for sample AE01036 processed on January 22 and 23, 2002.

NYC-WTC_000003249–000003325

Folder label: “524 1/22/02

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Scanned page image, NYC-WTC_000003285
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02JAN22\00917.D Vial: 12 Acq On : 22 Jan 2002 6:34 pm Operator: Sample : nyc Inst : 210 Misc : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP010802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 4 Cyclotrisiloxane, hexamethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 21.09 0.10 ug/L 28589 1,4-DIFLUOROBENZENE 17.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 Cyclotrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 64 2 2-Methyl-7-phenylindole 207 C15H13N 000000-00-0 40 3 3-Methyl-2-phenylindole 207 C15H13N 010257-92-8 9 4 Arsenous acid, tris(trimethylsilyl) 342 C9H27AsO3Si3 055429-29-3 9 idance Scan 1558 (21.094 min): 00917.D(-) m Z 206.95 100 .00% 27

5000

96 40 133 191 20.80 21.00 21.20 21.40 59 119 m z 95.9S 20.02 20 40 60 80 100 120 140 160 180 200 220 idance #27918: Cyclotrisiloxane, hexamethyl- 27

5000 20.80 21.00 21.20 21.40 m z 208.05 1/.186 ss 191 15 133 73 119 163 177 222 20 40 60 80 100 120 140 160 180 200 220 ~dance #24652: 2-Methyl-7-phenylindole 27

20.80 21.00 21.20 21.40 5000 m Z 5

30 102 7688 165 178 191 > 20 40 60 80 100 120 140 160 180 200 220 dance #24653: 3-Methyl-2-phenylindole 2 7 20.80 21.00 21.20 21.40 m/z 208.95 11.33w

5000

130 77 102 178 191 > 20 40 60 80 100 120 140 160 180 200 220 20.80 21.00 21.20 21.40

00917.D HP010802.M Wed Jan 23 09:42:02 2002 Page 4

NYC-WTC 000003285

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NYC-WTC_000003285Source: NYC Law Department, mirrored locally

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