WTC sample cover sheet, Dec 12 2001

NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\01DEC12\1212C10.D Vial: 2 Acq On : 12 Dec 2001 9:07 am Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Misc : December 12, 2001 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Dec 12 9:45 2001 Quant Results File: HP120301.RES

Quant Method : C:\HPCHEM\1\METHODS\HP120301.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Tue Dec 04 11:24:20 2001 Response via : Initial Calibration DataAcq Meth : HP120301

Compound R.T. Qlon Response Conc Unit Qvalue ------------------------------------------------------------------------- 34) 2-CHLOROETHYL VINYL ETHER 17.21 63 128998 11.03 91 ug/L

35) MIBK 17.30 58 75286 10.76 ug/L 85 36) CIS-1,3-DICHLOROPROPENE 17.82 75 542120 11.58 99 ug/L

37) TOLUENE 18.59 91 1540085 11.10 100 ug/L

38) TRANS-1,3-DICHLOROPROPENE 18.85 75 415638 11.67 97 ug/L

39) 1,1,2-TRICHLOROETHANE 19.25 97 278256 11.48 98 ug/L

40) TETRACHLOROETHENE 20.02 166 428277 10.84 97 ug/L

41) 1,3-DICHLOROPROPANE 19.77 76 520936 11.70 96 ug/L

42) DIBROMOCHLOROMETHANE 20.47 129 371437 11.07 ug/L 97 43) 1,2-DIBROMOETHANE 20.91 107 258580 10.93 ug/L 99 44) CHLOROBENZENE 21.80 112 995500 10.61 99 ug/L

45) 1,1,1,2-TETRACHLOROETHANE 21.83 131 383524 10.70 94 ug/L

46) 2-HEXANONE 19.15 43 168702 11.73 98 ug/L

47) ETHYLBENZENE 21.83 91 1877493 11.22 98 ug/L

48) P & M-XYLENE 21.99 106 1309522 23.04 98 ug/L

49) O-XYLENE 22.96 91 1497556 11.72 ug/L 98 50) STYRENE 23.02 104 979146 11.62 ug/L 99 51) 1,1,2,2-TETRACHLOROETHANE 24.04 83 304282 12.34 ug/L 99 53) BROMOFORM 23.89 173 182780 11.08 ug/L 98 54) ISOPROPYLBENZENE 23.69 105 1569253 11.43 ug/L 99 55) 1,2,3-TRICHLOROPROPANE 24.37 110 96757 11.19 ug/L 100 56) N-PROPYLBENZENE 24.55 91 2141441 11.39 ug/L 99 57) BROMOBENZENE 24.79 156 399589 10.74 ug/L 83 58) 1,3,5-TRIMETHYLBENZENE 24.86 105 1484119 11.43 ug/L 99 59) 2-CHLOROTOLUENE 25.04 91 1454751 11.44 ug/L 98 60) 4-CHLOROTOLUENE 25.11 91 1397311 11.41 ug/L 96 61) TERT-BUTYLBENZENE 25.66 119 1282909 11.68 ug/L 96 62) 1,2,4-TRIMETHYLBENZENE 25.75 105 1546559 11.65 ug/L 97 63) SEC-BUTYLBENZENE 26.12 105 1683946 11.32 ug/L 98 64) P-ISOPROPYLTOLUENE 26.38 119 1305525 11.44 ug/L 99 65) 1,3-DICHLOROBENZENE 26.74 146 737920 10.99 ug/L 98 66) 1,4-DICHLOROBENZENE 26.95 146 768803 10.75 ug/L 97 67) N-BUTYLBENZENE 27.27 91 1444094 11.38 ug/L 99 68) 1,2-DICHLOROBENZENE 27.81 146 643513 11.25 ug/L 98 69) 1,2-DIBROMO-3-CHLOROPROPAN 29.58 157 30216 11.83 ug/L 84 70) 1,2,4-TRICHLOROBENZENE 31.88 180 395168 11.18 ug/L 96 71) HEXACHLOROBUTADIENE 32.18 225 277714 10.57 ug/L 96 72) NAPHTHALENE 32.72 128 493147 12.06 ug/L 98 73) 1,2,3-TRICHLOROBENZENE 33.44 180 332424 11.32 ug/L 98 74) NITROBENZENE 29.79 77 182147 210.91 ug/L 95

------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 1212C10.D HP120301.M Fri Dec 14 09:16:09 2001 Page 2

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