WTC sample cover sheet, Dec 7 2001

NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\01dec07\1207R40A.D Vial: 5 Acq On 7 Dec 2001 4:00 pm Operator: 201-wb Sample : ref 40 Inst : GC/MS Ins Misc : December 6, 2001 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Dec 7 16:38 2001 Quant Results File: HP120301.RES

Quant Method : C:\HPCHEM\1\METHODS\HP120301.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Tue Dec 04 11:24:20 2001 Response via : Initial Calibration DataAcq Meth : HP120301

Compound R.T. Qlon Response Conc Unit Qvalue ------------------------------------------------------------------------- 35) MIBK 17.37 58 312556 39.33 ug/L 88 36) CIS-1,3-DICHLOROPROPENE 17.89 75 2182389 41.03 ug/L 99 37) TOLUENE 18.66 91 5298233 33.62 ug/L 97 38) TRANS-1,3-DICHLOROPROPENE 18.94 75 1730103 42.78 ug/L 98 39) 1,1,2-TRICHLOROETHANE 19.32 97 953798 34.65 ug/L 100 40) TETRACHLOROETHENE 20.10 166 1527602 34.03 ug/L 97 41) 1,3-DICHLOROPROPANE 19.84 76 1870294 36.99 ug/L 99 42) DIBROMOCHLOROMETHANE 20.54 129 1465605 38.47 ug/L 98 43) 1,2-DIBROMOETHANE 20.99 107 1054007 39.21 ug/L 99 44) CHLOROBENZENE 21.88 112 3595513 33.74 ug/L 99 45) 1,1,1,2-TETRACHLOROETHANE 21.92 131 1471392 36.13 ug/L 98 46) 2-HEXANONE 19.21 43 688764 42.16 ug/L 100 47) ETHYLBENZENE 21.92 91 6695057 35.22 ug/L 98 48) P & M-XYLENE 22.07 106 4616501 71.50 ug/L 96 49) O-XYLENE 23.05 91 5515523 38.00 ug/L 97 50) STYRENE 23.10 104 3624415 37.86 ug/L 99 51) 1,1,2,2-TETRACHLOROETHANE 24.13 83 1029774 36.76 ug/L 99 53) BROMOFORM 23.97 173 744907 41.92 ug/L 98 54) ISOPROPYLBENZENE 23.76 105 5914386 39.99 ug/L 100 55) 1,2,3-TRICHLOROPROPANE 24.46 110 358206 38.47 ug/L 100 56) N-PROPYLBENZENE 24.63 91 7751587 38.28 ug/L 100 57) BROMOBENZENE 24.88 156 1476359 36.82 ug/L 91 58) 1,3,5-TRIMETHYLBENZENE 24.95 105 5300061 37.91 ug/L 98 59) 2-CHLOROTOLUENE 25.12 91 5263590 38.41 ug/L 99 60) 4-CHLOROTOLUENE 25.19 91 4802587 36.40 ug/L 99 61) TERT-BUTYLBENZENE 25.75 119 4786263 40.45 ug/L 97 62) 1,2,4-TRIMETHYLBENZENE 25.84 105 5456448 38.15 ug/L 97 63) SEC-BUTYLBENZENE 26.20 105 6323990 39.47 ug/L 99 64) P-ISOPROPYLTOLUENE 26.46 119 4882861 39.73 ug/L 98 65) 1,3-DICHLOROBENZENE 26.83 146 2615369 36.16 ug/L 98 66) 1,4-DICHLOROBENZENE 27.04 146 2654401 34.44 ug/L 97 67) N-BUTYLBENZENE 27.35 91 5317154 38.91 ug/L 99 68) 1,2-DICHLOROBENZENE 27.89 146 2280031 36.99 ug/L 95 69) 1,2-DIBROMO-3-CHLOROPROPAN 29.67 157 137153 49.85 ug/L 80 70) 1,2,4-TRICHLOROBENZENE 31.99 180 1596691 41.93 ug/L 98 71) HEXACHLOROBUTADIENE 32.28 225 1080773 38.20 ug/L 98 72) NAPHTHALENE 32.82 128 1976961 44.90 ug/L 97 73) 1,2,3-TRICHLOROBENZENE 33.54 180 1303797 41.22 ug/L 94 74) NITROBENZENE 29.90 77 891812 958.66 ug/L 98

------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 1207R40A.D HP120301.M Fri Dec 07 16:38:49 2001 Page 2

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