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Chain of Custody: DEP Cleanup Samples, October 24, 2002

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Chain of custody document from PSC Analytical Services regarding the receipt and analysis of samples for the DEP cleanup project.

NYC-WTC_000130104–000130402
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NYC 9/11 Public Portal Document

PSC Analytical Services Certificate of Analysis R02090971 R02090971 R02090971 R02090971 Client ID: 05A 06A 07A 08A Lab No.: 039323 02 039324 02 039325 02 039326 02 Date Sampled: 02/09/12 02/09/12 02/09/12 02/09/12 Component MDL Units

Total Tetrachlorodibenzofurans pg 140 210 3.1 200 Total Pentachlorodibenzofurans 70 110 <0.55 56 Total Hexachlorodibenzofurans 33 70 <0.66 19 Total Heptachlorodibenzofurans 2.5 91 <0.84 <0.33 Octachlorodibenzofuran 4.4 38 <2.4 20 Total Tetrachlorodibenzo-p-dioxins 130 190 <0.65 200 Total Pentachlorodibenzo-p-dioxins 130 97 1.1 70 Total Hexachlorodibenzo-p-dioxins 93 190 1.1 70 Total Heptachlorodibenzo-p-dioxins 51 490 5.9 84 Octachlorodibenzo-p-dioxin 120 2000 17 280 Internal Recoveries % 2,3,7,8-T4CDF-13C12 83 80 86 87 2,3,7,8-T4CDD-13C12 84 84 83 86 1,2,3,7,8-P5CDF-13C12 71 65 81 79 1,2,3,7,8-P5CDD-13C12 75 73 90 90 1,2,3,6,7,8-H6CDF-13C12 58 46 80 71 1,2,3,6,7.8-H6CDD-13C12 71 67 81 81 1,2,3,4,6,7,8-H7CDF-13C12 56 39 52 78 1,2,3,4,6,7,8-H7CDD-13C12 79 81 91 88 OCDD-13C12 74 78 77 80

2,3,7,8-C14-Dibenzofuran (DB5) pg 40 55 1.6 42 2,3,7,8-C14-Dibenzo-p-dioxin 14 <20 <0.71 14 1,2,3,7,8-CI5-Dibenzofuran 6.4 11 <0.55 5.8 2,3,4.7.8-C15-Dibenzofuran 8.7 14 <0.53 <7.3 1,2,3,7,8-CI5-Dibenzo-p-dioxin <2.8 3.9 <0.48 2.2 1,2,3,4,7,8-CI6-Dibenzofuran 14 28 <0.61 <12 1,2,3,6,7,8-CI6-Dibenzofuran <6.3 <12 <0.58 <5.9 2,3,4,6,7,8-C16-Dibenzofuran 7.3 15 <0.66 6.2 1,2,3,7,8,9-C16-Dibenzofuran 1.1 <3.6 <0.73 <1.5 1,2,3,4,7,8-CI6-Dibenzo-p-dioxin <1.7 3.4 <0.68 1.3 1,2,3,6,7,8-C16-Dibenzo-p-dioxin 3.4 9.5 <0.64 2.8 1,2,3,7,8,9-C16-Dibenzo-p-dioxin 5.8 13 <0.63 4.0 1,2,3,4,6.7.8-CI7-Dibenzofuran <30 91 <6.6 <60 1,2,3,4,7,8,9-CI7-Dibenzofuran <3.4 <14 <5.4 <5.7 1,2,3,4,6,7,8-CI7-Dibenzo-p-dioxin 22 220 2.4 36 1,2,3,4,6,7,8,9-CI8-Dibenzofuran 4.4 38 <2.4 20 1,2,3,4,6,7,8,9-CI8-Dibenzo-p-dioxin 120 2000 17 280

2,3,7,8-TCDF (DB225) pg 7.3 9.9 <2.0 12 Internal Recoveries % 2,3,7,8-TCDF-13C12 116 111 111 112

TEO based on Nato Factors pg 26 27 0.20 22

Certificate No:2J0631 file # =R02090971 revised TEQ final Report.xls nh Page 2 of 3 Revision No. 0

NYC-WTC 000130137

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NYC-WTC_000130052 · Box DEP Box 53

Chain of custody document from PSC Analytical Services regarding the receipt and analysis of samples for the DEP cleanup project.

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