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Chain of Custody: DEP Cleanup Samples, October 24, 2002

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Chain of custody document from PSC Analytical Services regarding the receipt and analysis of samples for the DEP cleanup project.

NYC-WTC_000130104–000130402
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NYC 9/11 Public Portal Document

PSC Analytical Services Certificate of Analysis R02090971 R02090971 R02090971 R02090971 Client ID: 12A 02A 03A 04A Lab No.: 039319 02 039320 02 039321 02 039322 02 Date Sampled: 02/09/12 02/09/12 02/09/12 02/09/12 Component MDL Units

Total Tetrachlorodibenzofurans pg 18 57 100 4.2 Total Pentachlorodibenzofurans 3.5 8.6 31 0.45 Total Hexachlorodibenzofurans 13 4.3 16 <0.50 Total Heptachlorodibenzofurans <2.1 <4.8 <1.4 <3.3 Octachlorodibenzofuran 9.7 4.0 5.0 <0.82 Total Tetrachlorodibenzo-p-dioxins 11 36 120 2.4 Total Pentachlorodibenzo-p-dioxins 5.1 12 64 0.88 Total Hexachlorodibenzo-p-dioxins 7.8 14 58 1.7 Total Heptachlorodibenzo-p-dioxins 24 17 35 <0.51 Octachlorodibenzo-p-dioxin 89 54 74 8.4 Internal Recoveries % 2,3,7,8-T4CDF-13C12 85 72 71 85 2,3,7,8-T4CDD-13C12 82 73 70 88 1,2,3,7,8-P5CDF-13C12 54 48 59 70 1,2,3,7,8-P5CDD-13C12 52 49 65 88 1,2,3,6,7,8-H6CDF-13C12 28 31 49 28 1,2,3,6,7,8-H6CDD-13C12 48 62 83 55 1,2,3,4,6,7,8-H7CDF-13C12 17 20 39 13 1,2,3,4,6,7,8-H7CDD-13C12 54 64 77 74 OCDD-13C12 54 65 82 70

2.3,7,8-CI4-Dibenzofuran (DB5) pg 0.44 <0.23 33 2.3 2,3,7,8-CI4-Dibenzo-p-dioxin <0.75 <0.34 <0.55 <0.52 1,2,3,7,8-C15-Dibenzofuran <2.5 2.4 5.2 <0.58 2,3,4,7,8-C15-Dibenzofuran <2.3 <2.4 5.3 0.45 1,2,3,7,8-CI5-Dibenzo-p-dioxin <1.1 <0.99 1.9 <0.48 1,2,3,4,7,8-CI6-Dibenzofuran <5.6 4.3 9.6 <0.44 1,2,3,6,7,8-CI6-Dibenzofuran <3.7 <3.1 <3.9 <0.44 2,3,4,6,7,8-CI6-Dibenzofuran 6.3 <5.4 <4.3 <0.50 1,2,3,7,8,9-C16-Dibenzofuran 6.4 <0.96 1.5 <0.56 1.2,3.4,7,8-CI6-Dibenzo-p-dioxin <2.4 <0.40 1.1 <0.41 1.2,3,6,7,8-CI6-Dibenzo-p-dioxin 2.7 <1.2 2.7 <0 41 1,2,3,7,8,9-CI6-Dibenzo-p-dioxin 5.1 <3.2 3.1 <0.39 1,2,3,4,6,7,8-C17-Dibenzofuran <1.9 <3.5 <53 <130 1,2,3,4,7,8,9-CI7-Dibenzofuran <16 <9.9 <1.4 <15 1,2,3,4,6,7,8-CI7-Dibenzo-p-dioxin 16 9.8 15 <1.1 1,2,3,4,6,7,8,9-C18-Dibenzofuran 9.7 4.0 5.0 <0.82 1,2,3,4,6,7,8,9-CI8-Dibenzo-p-dioxin 89 54 74 8.4

2.3,7,8-TCDF (DB225) pg <3.0 3.9 4.8 <2.7 Internal Recoveries % 2,3,7,8-TCDF-13C12 118 112 107 111

TEQ based on Nato Factors pg 2.4 0.71 9.1 0.47

Certificate No:2J0631 file # =R02090971 revised TEQ final Report.xls nh Page 1 o/ 3 Revision No. 0

NYC-WTC 000130136

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NYC-WTC_000130052 · Box DEP Box 53

Chain of custody document from PSC Analytical Services regarding the receipt and analysis of samples for the DEP cleanup project.

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