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← Document results/DEP Box 37/250 BROADWAY; Block: 124 Lot: 24 BIN: 1001408 245 Broadway, 2-4 Murray St. 1-7 Park Pl, 239- 247 Broadway
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Background sampling chain of custody, 250 Broadway, Sept 2001

Machine-extracted title · confidence 90%

Chain of custody documentation for background sampling including asbestos and lead at 250 Broadway in September 2001.

NYC-WTC_000106077–000106100

Folder label: “250 BROADWAY; Block: 124 Lot: 24 BIN: 1001408 245 Broadway, 2-4 Murray St. 1-7 Park Pl, 239- 247 Broadway”

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NYC 9/11 Public Portal Document

2123533599 ATC ASSOCIATES INC PAGE 02/E . 09/17/2001 00:36

ATC ASSOCIATES INC. - NOB ANALYSIS Batch No. S ~ 11106/~ Grid Box No. Operator 1 !l Sample No. y `6 IIá ` / Grid I.D. 2410 Date /6 d

'=4-■■■ Ru- -I■■ ► I w - URuUR

F= Single Fiber (1-3 intersections = 1-3 fibers) AMPHIBOLE B= Bundle (:3 fibers <1 fiber diameter apart) Amosite C= Cluster >3 intersections) Crocidolit M= Matrix Anthophylb TremolitE NSD= No Structures Detected Actinolite

Positive diffraction pattern observed conforming to identification criteria For chrysotile: 7.3A spacing for 020 reflections (= 60urn objective aperture), 5.3A spacing for the layer -line repeat (= 1/3 60urn objective aperture), 110 an 130 streaks and presence of 002 and 200 reflections. For amph.iboles: 5.3A layer-line repeat and approximate 3.5 ratio of non-tirinn layer-line reflection spacing to layer-line repeat distance.

EDX spectrum observed conforming to identification criteria. Minimum Requirements: Identify 4 fibers by electron diffraction. Chrysotile: 5.3A layer-line (row) spacing with correct 020. 002. 110, 130 and 200 points or streaks. Amphibole: Correct 5.3A layer-line spacing. EDX Requirements: Chrysotile: none. ' Ampbibole: identify amphibole species by EDX.

QVANTTTATX0N: Estimated Percent Asbestos on: Grid 1: Grid 2: Mean (N): Percent Asbestos in Subsample: (N X K)/G:

From PLM NOB ANALYSIS SHEET: 10 X 11 = 14 where 10 = total residue %. ii. = residue asb % TEM and 14 = total % asb & is Also, 1% total asbestos = 100/total residue %. tt\3ALA~ P=vAS11ta3z%c►Dc% X *M3D

NYC-WTC 000106094

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NYC-WTC_000106094Source: NYC Law Department, mirrored locally

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