P1 ATC ASSOCIATES INC. - TEM ANALYSIS
LAB GROUP d 5'0? - 3/ 4/0L
/
r
Lao Sample No. 52545 Filter ..pe MCE 35 mm Cnerst~: `- L'-?~
Client Spl. No 39 Fisher Area 340 min'2
/_
Instrument I.D EM 10 CRY. Grid I.D. DISK No
Screen Magnification 15,400: {001 Area 3.01 1 mrn'3 Crmments
Arc. Voltage 80 kV No. GC to be Analysed 5 4 ' S`r'c_. _oracc. 7 s'mm"=
GO. Structure Structure Type Length I I.D. of Structure EDS
N or s/ !
>,U.S um (Nonasb.
No Coord. No. F H C M >. 5urn Chrysd Amphibole Nonasb. Ambig./NDI Elements)
< 5um
rr2
2-
3 /~~ — C~
7
J T —e,
I
I
I
I
1
1
I
Photo No. (from 1 in 5 asbestos- Identify all structures usin EDS Check diffraction for asbestos Store all unrepeated spectra
containing samples) iGrid acceptance: structures u to 70s t?ftm (1st 4)
I Strict = > 0.5um & > 5:1 Aspect Ratio <50z undiesolve t er, overlapped or folded
<10% particulate coverage >50% coverage Totals
N= Not Observed (EDS spectrum or diffraction pattern) at least 20 unfolded or overlapped grid squares
<5% holes or o a ue areas
Positive diffraction pattern properties conforming F B C M - 5um
to laboratory Identification criteria observed. Unused portion
For chrysoille: 0.73nm spacing for (020) reflections, of (liter
0.53em spacing for the layer line repeat, streaking Chrysotile
Avoided portion
of (110) and (190) reflections. of filter
For amphiboles: 0.53nm layer line repeat, and apprea. Pvrtlon of (liter (2mm side)
2.5 ratic of non-t>rtnnetl layer Itne spot spacing m
esamQna in
Amphibole
layer line repeat distance (0.59am).
EDS spectrum conforming to laboratory
identification criteria observed. AMPHIBOLES Ambiguous
F= Single Fiber (1-3 intersections = 1-3 fibers) Amosite
8= Bundle (>3 fibers <1 fiber diameter apart)
C= Cluster (>3 intersections)
25mm inter Crocidolite Non —asbestos!
M= Matrix Stopping Bukas: Anthophyllite
NSD= No structure. Detected >50 ./c.o. or in at. 4 G.o. I Tremalite
Actinolite Non —Identified ~'
L•\0ATA\PlUVATE\XIKEG\CADD\1'ZM3 9/22/98
NYC-WTC 000104306
OCR can misread numbers and units. Confirm readings against the page image before using them.
NYC-WTC_000104306Source: NYC Law Department, mirrored locally
Technical data sheet recording microscopic analysis parameters and structural identification for asbestos fiber samples analyzed by transmission electron microscopy.