ATC ASSOCIATES INC. - TEM ANALYSIS
LAB GRCUP d. 5'59 - 1) 26/0.
I Filter Type MCE 3_ mm ODera Ccr
Lab Sample Mc. 5253i
Client Spl. No 32 Filter Area 385 mm"2
Grid I.C. v & Disk No.
Instrument I.D. EM L CAN
Screen Magnification 15,400X (GO) Area 0.01134 mm'. Commer.ts
Acc. Voltage 80 kV No. GO tc be Analyzed i 4 '21 Struc: Ccrsrd. :o 'L s'mm"3
EDS
GO. Structure structure Type Length I.D. of Structure N or
(Nonasb.
I No Coord. No. F B C M <05 5um Chrys. Amphibole Nonasb. Ambig./NDi Elements)
I
I
I
J
H
Photo No. (from 1 in 5 asbestos— Identify all structures using EDS Check diffraction for asbestos Store all unrepeated spectra
containing samples) Grid acceptance: structures u to 70a t~tim ( let 4)
<50% undissolve i r• pe r b e
Struct. = > C.5um & > 5:1 Aspect Ratio Totals
<10% particulate coverage >50% coverage
N= Not Observed (EDS spectrum or diffraction pattern) lat least 20 unfolded or overlapped grid squares
<5S holes or opaque areas
Positive diffraction pattern properties conforming
to laboratory identification criteria Unused portion
Far aha7aoUle: a.73nm spacing for (020) renectiona. of filter Chrysotile
0.9.7am spacing for the layer line repeat, streaking Avoided portion
of (110) and (130) reflections. of filter
Par amphibalas: 0.59nm layer line repeat. and approx. (2mm olds)
3.5 ratio of non-twinned In line spot spacing to Amphibole
Layer line repeat distance (a.07nm).
✓= EDS spectrum conforming to laboratory Ambiguous
I identification criteria observed. PHIBOLES
observed.e7Arnosite
Fa Single Fiber (1-3 intersections = 1-3 fibers)
B= Bundle (>3 fibers <1 fiber diameter apart) 22mm niter Crocidolite Non —asbestos
C= Cluster >3 intersections) ''--~ Rules: Anthophyllite
M= Matrix Stopping
NSD No Structures Detected >5a a/C.o. or in 1st 4 C.O. I Tremolite
Actinolite Non —Identified
I L.\0ATA\PRIVATE\MIKEC\CADDytM3 9/22/98
NYC-WTC 000104299
OCR can misread numbers and units. Confirm readings against the page image before using them.
NYC-WTC_000104299Source: NYC Law Department, mirrored locally
Laboratory report documenting transmission electron microscopy analysis of asbestos samples collected from a New York City Department of Education site in October 2001.