ATC ASSOCIATES INC. - TEM ANALYSIS
LAB GROUP #. 5 - 09 -
Lab Sample Nc. 52525 F:icer Type MCE 25 mm Operator
Client Spi. No. 19 Filter Area 385 mm-2
Instrument I.D. EM 10 CP.X Grid 1.0 DISK No.
Screen Magnification 14. 400X (GOB Area 7.)1_24 mm'_ Comments
Acc Voltage 80 kV No. GO cc be Pnaiyzed 4 7 S_rucc Ccrsod, cc s'mm"2
Structure Structure Type Length I.D. of Structure EDS
I GO. N or,/
(Nonasb.
INo Coord. No. F B C M >0.5
< 5 um
um >, 5am Chrys. Amphibole Nonasb. Ambig./ND Elements)
c`
I,; .J
i _7 — cs
I
I
I
I
I
D Photo No. (from 1 in 5 asbestos- IdenLify all structures usin EDS Check diffraction for asbestos Store all unrepeated spectra -
containing samples) Grid acceptance: structures u to 70s f~tm (lot 4)
Struct. _ > 0.Sum & > 5:1 Aspect Ratio <50x undlssoive i er, overappe or o e
<10% particulate coverage >50% coverage Totals
N= Not Observed (Ens spectrum or diffraction pattern) pat least 20 unfolded or overlapped grid squares
<5% holes or o a tie areas
Positive diffraction pattern properiles conforming
La laboratory identification criteria observed. Unused portion
Par chrysoUls: 0.73nm apacin( for (020) reneetiona,
0.53nm apameg for the Mayer line repast.
as streak.ag
of filter Chrysotile
Avoided pardon
of (110) and (130) reflections. of filter
For amphiboles: O.5Dnm layer line repeat. and approx. PorUon of filter (2mm wide)
3.5 ratio of non-twinned layer line spot spacing to subject Io
ezammaUon
Amphibole
layer line repeat distance (0.57nm).
EDS spectrum conforming to laboratory Ambiguous
Identification criteria observed. AMPHIBOLES
F= Single Fiber (1-3 intersections = 1-3 fibers) Amosite
8= Bundle (>3 fibers <l fiber diameter apart)
Cluster (>3 intersections)
25mm filter i Crocidolite Non-asbestos
Stepping Rule.: Anthophyllite
MaUls
NSD= No Structures Detected >50 5/G.0. or in let 4 0.0. Tremolite
C=
Iii
Actinoiitc
Non -Identified
L`DATA\PRIVATE\MIKEG\CADOVEM7 8/22/98
NYC-WTC 000104286
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