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Document / 7 pages

Pesticide method validation data, Dec 2001

Machine-extracted title · confidence 90%

Technical document presenting method validation statistics including average response and relative standard deviation for pesticide analysis.

NYC-WTC_000092394–000092400

Folder label: “508 X 11/5/01 A 12/1/01

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Scanned page image, NYC-WTC_000092399
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document (^uancicacion Keporc tUT Keviewea;

Signal #1 : C:\MSDCHEM\1\DATA\5O8\O112O1\PESTUR.D\ECD1A.CH Vial: 9 'Signal #2 : C:\MSDCHEM\1\DATA\508\011201\PESTUR.D\ECD2B.CH Acq On : 01 Dec 2001 6:35 pm Operator: Nefliu Sample : pest unextracted ref Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 12 11:17:03 2001 Quant Results File: 011203P.RES

Quant Method : C:\MSDCHEM\1\METHODS\011203P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Mon Dec 03 10:48:55 2001 Response via : Initial Calibration DataAcq Meth : 508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Compound RT#1 RT#2 Resp#l Resp#2 ug/1 , ug/1

System Monitoring Compounds

Target Compounds Propachlor 9.18 8.60 76687655 59817137 0.180^^/- 0.185 1) 2) g-BHC 9.96 10.27 904.0E6 786.3E6 0.137'^1-/. 0.137 3) Heptachlor 11.12 11.32 501.3E6 366.5E6 0.089/9/. 0.091 4) Aldrin 11.83 12.06 273.6E6 250.0E6 0.044/// 0.044 5) Heptachlor Epoxi 13.26 13.41 754.9E6 699.2E6 0.1389a.y- 0.139 6) 4,4-DDE 14.09 14.62 2015.1E6 1915.4E6 0.391^//. 0.395 7) Dieldrin 14.68 14.88 397.5E6 368.2E6 0.071/9/ 0.074 8) Endrin 15.18 15.54 278.7E6 287.9E6 0.080m/j?/ 0.083 9) Methoxychlor 17.12 18.08 333.5E6 245.5E6 0.183m^jt^ 0.180

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. PESTUR.D 011203P.M Wed Dec 12 11:18:03 2001 Page 1

NYC-WTC_000092399

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NYC-WTC_000092399Source: NYC Law Department, mirrored locally

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