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Pesticide and PCB analysis results, sample AD26532, Nov-Dec 2001

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Laboratory analysis of sample AD26532 for organochlorine pesticides and PCBs, tested Nov 6-Dec 1, 2001; multiple analytes detected including Lindane, Heptachlor, and 4,4-DDE.

NYC-WTC_000091121–000091124

Folder label: “508 X 11/6/01 A 12/1/01

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NYC 9/11 Public Portal Document (^uaiicicacxori Keporc Keviewea;

Signal #1 : C:\MSDCHEM\l\DATA\508\011201\1106RPC.D\ECDlA.CH Vial: 13 Signal #2 : C:\MSDCHEM\l\DATA\508\011201\1106RPC.D\ECD2B.CH Acq On : 01 Dec 2001 8:29 pm Operator: Nefliu Sample : 11/06 ref pest-chl Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 12 11:22:36 2001 Quant Results File: 011203P.RES

Quant Method : C:\MSDCHEM\1\METHODS\011203P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Mon Dec 03 10:48:55 2001 Response via : Initial Calibration DataAcq Meth : 508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal '#2 Info : Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.46 15.05 468.3E6 419.3E6 0.165m 0.167m Spiked Amount 0.200 Recovery ‘ = 82.50% 83.50% Target Compounds 1) Propachlor 9.18 8.60 113.5E6 92183777 0.267 0.285 2) g-BHC 9.95 10.27 1527.3E6 1377.0E6 0.232 0.240 3) Heptachlor 11.12 11.32 731.4E6 562.9E6 0.130 0.139 4) Aldrin 11.82 12.06 168.0E6 158.5E6 0.027 0.028 5) Heptachlor Epoxi 13.26 13.41 1432.5E6 1233.5E6 0.262 0.246 6) 4,4-DDE 14.09 14.62 2692.5E6 2599.8E6 0.522 0.536 7) Dieldrin 14.67 14.88 748.3E6 750.2E6 0.133 0.150 8) Endrin 15.18 15.54 676.2E6 674.0E6 0.195 0.193 9) Methoxychlor 17.11 18.08 652.4E6 538.5E6 0.358rn 0.394m

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 1106RPC.D 011203P.M Wed Dec 12 11:23:49 2001 Page 1

NYC-WTC_000091123

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NYC-WTC_000091123Source: NYC Law Department, mirrored locally

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