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Pesticide method validation data, Dec 2001

Machine-extracted title · confidence 90%

Technical document presenting method validation statistics including average response and relative standard deviation for pesticide analysis.

NYC-WTC_000092394–000092400

Folder label: “508 X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document / < Response Factor Report Instrumen

Metfiod : C:\MSDCHEM\1\METHODS\011203P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Mon Dec 03 10:48:55 2001

Calibration Files 1 =PESTC1.D 2 =PESTC2.D 3 =PESTC3.D TA 4—

Compound 1 2 3 Avg %RSD

1) Propachlor 4.843 4.166 3.757 4.255 E8 12.89 2) g-BHC 6.432 6.595 6.716 6.581 E9 2.16 3) Heptachlor 5.670 5.446 5.735 5.617 E9 2.70 4) Aldrin 6.114 6.167 6.357 6.213 E9 2.06 5) Heptachlor Epoxide 5.485 5.428 5.469 5.461 E9 0.53 6) 4,4-DDE 5.022 5.196 5.261 5.160 E9 2.39 7) Dieldrin 5.623 5.554 5.674 5.617 E9 1.07 8) Endrin 3.363 3.446 3.604 3.471 E9 3.52 9) Methoxychlor 1.859 1.803 1.809 1.823 E9 1.70 10) s 2,4-DDD SURROGATE 2.834 2.834 E9 0.00

Signal #2 Calibration Files 1 =C01N01.D 2 =C02N01.D 3 =C03N01.D- Compound 1 2 3 Avg %RSD

1) Propachlor 3.580 3.185 2.923 3.229 E8 10.24 2) g-BHC 5.353 5.829 6.023 5.735 E9 6.02 3) Heptachlor 3.996 3.910 4.243 4.050 E9 4.28 4) Aldrin 5.307 5.781 5.970 5.686 E9 6.01 5) Heptachlor Epoxide 4.956 5.023 5.058 5.013 E9 1.03 6) 4,4-DDE 4.632 4.923 4.984 4.846 E9 3.89 7) Dieldrin 4.580 5.086 5.310 4.992 E9 7.49 8) Endrin 3.278 3.520 3.667 3.488 E9 5.64 9) Methoxychlor 1.349 1.352 1.398 1.367 E9 1.99 10) s 2,4-DDD SURROGATE 2.518 2.518 E9' 0.00

(#) = Out of Range 011203P.M Tue Dec 18 10:40:36 2001 Page 1

NYC-WTC_000092394

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NYC-WTC_000092394Source: NYC Law Department, mirrored locally

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