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← Document results/DEP Box 68/508 X 12/21/01 A 1/3/02
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DEP Lab Results: Pesticide CCV2 Analysis, Sample AD31072

Machine-extracted title · confidence 90%

Calibration verification data for pesticide analysis of sample AD31072 showing recovery percentages in January 2002.

NYC-WTC_000090533–000090539

Folder label: “508 X 12/21/01 A 1/3/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\l\DATA\508\020103C\2TOXC2.D\ECDlA.CHVial: 56 Signal #2 : C:\MSDCHEM\1\DATA\508\020103C\2TOXC2.D\ECD2B.CH Acq On 04 Jan 2002 4:57 pm Operator Nefliu Sample tox cev Inst Instrumen Mise : Multiplr 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Jan 07 08:50:02 2002 Quant Results File: 020103T.RES

Quant Method C:\MSDCHEM\1\METHODS\020103T.M (Chemstation Integrator) Title 508 Chlorinated Pesticides - Toxaphene Last Update Fri Jan 04 11:09:38 2002 Response via Initial Calibration DataAcq Meth MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 Conc#l Conc#2

System Monitoring Compounds 6) s 2,4-DDD SURROGAT 14.36 14.97 623.8E6 498.2E6 0.179m 0.189m Spiked Amount 0.200 Recovery 89.50% 94.50%

Target Compounds 1) Toxaphene Peak 1 14.77 15.70 117.0E6 72332399 2.867m 3.065m 2) Toxaphene Peak 2 15.14 16.12 217.9E6 390.2E6 2.808m 3.308m 3) Toxaphene Peak 3 15.55 16.28 112.6E6 121.5E6 2.764m 3.090m 4) Toxaphene Peak 4 17.20 16.70 508.3E6 359.5E6 2.931m 3.226m 5) Toxaphene Peak 5 17.58 17.78 196.4E6 444.4E6 2.804m 3.279m

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 2TOXC2.D 020103C.M Mon Jan 07 10:56:18 2002 Page 1

NYC-WTC_000090538

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NYC-WTC_000090538Source: NYC Law Department, mirrored locally

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