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Document / 4 pages

Organochlorine pesticide analysis results, sample AD27143, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report listing detection levels for multiple organochlorine pesticides including Toxaphene in sample AD27143.

NYC-WTC_000090556–000090559

Folder label: “508 X 12/21/01 A 1/3/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 ■: C:\MSDCHEM\l\DATA\508\020103C\27143SDT.D\ECDlA.CHVial: 35 Signal #2 : C:\MSDCHEM\l\DATA\508\020103C\27143SDT.D\ECD2B.CH Acq On : 04 Jan 2002 6:52 am Operator: Nefliu Sample : 27143 spike dupe tox Inst : Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Jan 04 11:20:09 2002 Quant Results File: 020103T.RES

Quant Method C:\MSDCHEM\1\METHODS\020103T.M (Chemstation Integrator) Title 508 Chlorinated Pesticides - Toxaphene Last Update Fri Jan 04 11:09:38 2002 Response via Initial Calibration DataAcq Meth MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 Conc#l Conc#2

System Monitoring Compounds 6) s 2,4-DDD SURROGAT 14.36 14.97 592.7E6 443.4E6 0.170m 0.168m Spiked Amount 0.200 Recovery = 85.00% 84.00%

Target Compounds 1) Toxaphene Peak 1 14.78 15.72 181.5E6 40888061 4.448m 1.733m# 2) Toxaphene Peak 2 15.16 16.12 216.6E6 528.1E6 2.791m 4.477m# 3) Toxaphene Peak 3 15.55 16.28 365.8E6 98567271 8.978m 2.507m# 4) Toxaphene Peak 4 17.20 16.70 398.7E6 380.3E6 2.299m 3.412m# 5) Toxaphene Peak 5 17.58 17.78 105.9E6 337.6E6 1.512m 2.491m#

4:0

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 27143SDT.D 020103T.M Fri Jan 04 11:21:06 2002 Page 1

NYC-WTC_000090558

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NYC-WTC_000090558Source: NYC Law Department, mirrored locally

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