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← Document results/DEP Box 68/508 X 12/21/01 A 1/3/02
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Organochlorine pesticide analysis results, sample AD27143, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report listing detection levels for multiple organochlorine pesticides including Toxaphene in sample AD27143.

NYC-WTC_000090552–000090555

Folder label: “508 X 12/21/01 A 1/3/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\l\DATA\508\020103C\27143ST.D\ECDlA.CH Vial: 34 Signal #2 : C:\MSDCHEM\l\DATA\508\020103C\27143ST.D\ECD2B.CH Acq On : 04 Jan 2002 6:23 am Operator: Nefliu Sample : 27143 Spike tox Inst : Instrumen Mise ; Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Jan 04 11:21:14 2002 Quant Results File: 020103T.RES

Quant Method C:\MSDCHEM\1\METHODS\020103T.M (Chemstation Integrator) Title 508 Chlorinated Pesticides - Toxaphene Last Update Fri Jan 04 11:09:38 2002 Response via Initial Calibration DataAcq Meth MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 Conc#l Conc#2

System Monitoring Compounds 6) s 2,4-ODD SURROGAT 14.36 14.97 593.2E6 422.1E6 0.171m 0.160m Spiked Amount 0.200 Recovery 85.50% 80.00%

Target Compounds 1) Toxaphene Peak 1 14.78 15.72 186.9E6 38756274 4.580m 1.643m# 2) Toxaphene Peak 2 15.17 16.12 231.2E6 531.5E6 2.978m 4.505m# 3) Toxaphene Peak 3 15.55 16.28 361.9E6 102.5E6 8.883m 2.608m# 4) Toxaphene Peak 4 17.20 16.71 394.7E6 376.4E6 2.276m 3.377m# 5) Toxaphene Peak 5 17.58 17.78 100.1E6 333.8E6 1.429m 2.463m#

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 27143ST.D 020103T.M Fri Jan 04 11:22:14 2002 Page 1

NYC-WTC_000090554

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NYC-WTC_000090554Source: NYC Law Department, mirrored locally

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