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Document / 4 pages

Pesticide analysis results, sample AD27818, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report detailing pesticide concentrations and detection limits for sample AD27818 analyzed in January 2002.

NYC-WTC_000089904–000089907

Folder label: “508 X 1/7/02 A 1/10-1/11/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

/ Signal #1 : C:\MSDCHEM\l\DATA\508\020110B\0107REFT.D\ECDlA.CH Vial: 21 Signal #2 : C:\MSDCHEM\l\DATA\508\020110B\0107REFT.D\ECD2B.CH Acq On : 11 Jan 2002 9:56 am Operator: Nefliu Sample : 01/07 ref tox Inst Instrumen Miso : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: EVENTS2.E Quant Time: Jan 11 11:07:31 2002 Quant Results File: 020110T.RES

Quant Method : C:\MSDCHEM\1\METHODS\020110T.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides - Toxaphene Last Update : Fri Jan 11 08:14:26 2002 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 Conc#l Conc#2

System Monitoring Compounds 6) S 2,4-DDD SURROGAT 14.37 14.97 736.5E6 505.1E6 0.224m 0.206m Spiked Amount 0.200 Recovery = 112.00% 103.00%

Target Compounds 1) Toxaphene Peak 1 14.78 15.71 228.0E6 45681743 5.716m 1.975m# 2) Toxaphene Peak 2 15.16 16.12 285.6E6 584.2E6 3.742m 5.173m# 3) Toxaphene Peak 3 15.56 16.27 427.9E6 106.5E6 11.858m 2.738m# 4) Toxaphene Peak 4 17.21 16.’70 469.6E6 406.8E6 2.925m 3.789m# 5) Toxaphene Peak 5 17.59 17.78 109.9E6 370.3E6 1.786m 2.865m#

(f)=RT Delta >1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 0107REFT.D 020110T.M Fri Jan 11 11:08:39 2002 Page 1

NYC-WTC_000089906

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NYC-WTC_000089906Source: NYC Law Department, mirrored locally

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