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Toxaphene analysis results for samples TOXC1-3, Dec 2001

Machine-extracted title · confidence 90%

Chemical analysis report listing toxaphene compound concentrations and surrogate recovery metrics from December 2001.

NYC-WTC_000089559–000089567

Folder label: “508 X 11/27/01 A 12/4-12/26/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\508\011224B\TOXC2.D\ECD1A.CH Vial: 7 Signal #2 : C:\MSDCHEM\1\DATA\5 0 8\0112 2 4B\TOXC2.D\ECD2B.CH Acq On : 24 Dec 2001 3:34 pm Operator: Nefliu Sample : tox ic2 Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 31 15:17:51 2001 Quant Results File: 011224T.RES Quant Method : C:\MSDCHEM\1\METHODS\011224T.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides - Toxaphene Last Update : Wed Dec 26 10:40:08 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Compound RT#1 RT#2 Resp#l Resp#2 Conc#l Conc#2

System Monitoring Compounds 6) s 2,4-DDD SURROGAT 14.35 14.98 793.6E6 509.4E6 0.198m 0.192m Spiked Amount 0.200 Recovery 99.00% 96.00% Target Compounds 1) Toxaphene Peak 1 14.76 15.71 151.2E6 73624139 3.187m 3.241m 2) Toxaphene Peak 2 15.13 16.13 270.0E6 326.5E6 3.198m 2.939m 3) Toxaphene Peak 3 15.54 16.29 145.4E6 119.2E6 3.004m 3.173m 4) Toxaphene Peak 4 17.18 16.71 619.0E6 343.6E6 3.260m 3.183m 5) Toxaphene Peak 5 17.56 17.79 246.0E6 395.6E6 3.218m 3.163m

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. TOXC2.D 011224T.M Mon Dec 31 15:18:46 2001 Page 1

NYC-WTC_000089562

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NYC-WTC_000089562Source: NYC Law Department, mirrored locally

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