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GC/MS analysis report, sample AD23719, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23719 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089203–000089217

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089211
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23719.D Vial: 15 Acq On : 16 Oct 2001 1:53 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.39 0.40 ug/1 40426 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexaj26ne 100 C6H12O 000589-38-8 90. 2 2-ButXnone, 3,3 -dimethyl- 100 C6H12O 000075-97-8 32 3 CyclZpentanol, 3-methyl- 100 C6H12O 018729-48-1 28 4 2-/^Pentanedione _________________ 100 C5H8O2 000123-54-6 25 Abundance Scan 147 (6.387 min): 23719.D (-) m/z 4^/00 43 5|7

71 5000 100

85 6.00 6.20 6.40 6.60 6.80 I' I m/z 57700 95.66% nfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63358: 3-Hexanone 40 57

71 5000 6,00 6.20 6.40 6.60 6.80 100 m/z 71.00 56.19% +pTII|Ull|l 85 I"' ‘ I'"' r "' I ............... I TiZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63406: 2-Butanone, 3,3-dimelhyl-

41 6.00 6,20 6,40 6,60 6.80 5000 29 m/z 100.05 31.40% 100 15 TTrYpTirlrrTTyrrTrfTlT -- ------ 85- ......... I..... I"" 1 nZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63339: Cyclopentanol, 3-methyl- A........ - l S ,A, , , , , , , Y. ---- ” ------------ —~~ ------- ..7:1----- .6:00 -620 6:40~ aeo' "6(80 m/z. 41.05 22.60%

5000

44 82 r " ‘ r I 'I I" " I" " I IrrpTTpHTT-lTTTTp^TTJTTtTpT^^ . ...... . tVz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6.20 6.40 6.60 6.80

23719.D NP091101.M Tue Oct 16 15:14:22 2001 Page 1

“NYC-WTC_OOOO892H' '

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NYC-WTC_000089211Source: NYC Law Department, mirrored locally

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