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GC/MS analysis report, sample AD23719, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23719 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089203–000089217

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089213
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NYC 9/11 Public Portal Document

. Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23719.D Vial: 15 Acq On : 16 Oct 2001 1:53 am Operator: 2 09 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 6.74 0.50 ug/1 50606 1,4-Dichlorobenzene-d4 11.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H14O 000626-93-7 83 2 2-Pentanp2f, 4-methyl- 102 C6H14O 000108-11-2 74 3 2-Hexap61, (R)- 102 C6H14O ' 026549-24-6 64 4 2-He;e^ol, (S) -________________________ 102 C6H14O - 052019-78-0 64 Abundance Scan 185 (6.736 min): 23719.D (-) iriTz 44.95 100.00% 4|5

5000

41 69 55 „ I 8487 6.40 6.60 6.80 7.00 ''" I" I' 11 r.. I" " 11" 11.." 111" I... 11.1"," " I,. m/z 69.00 14.30% ■n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584: 2-Hexanol 4b

5000 . ......... 6.40 6.60 6.80 7.00 Xz 40.95 13747%

X Xx 8487 ................. ................. ........................ ti7z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63545:2-Pentanol, 4-methyl-______________________ 4)5 ' I ' ' ‘ ' I ' e.^ ' 6.^ ''e.so' 7.00 5000 m/z 43.00 10.73%

■n/z-> ^bundance 10 _27 --------- 394: ............................... 69 -------- 57----------- ----------------- 84^-- ... ........................... 11.......... 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #1794: 2-Hexanol, (R)- --------- ------------------------------ ST— 4t--------------------------- -- ---------------------------------------------’ xt "6:40 e^eoTZaso m/z44.00 JTZLJZLT— 7;oo. _ 8.24% 5000

69 55 I 84 87 ■ I " ’ ■ I ■ ” ■ I ‘' M " " I ’" ' I ’'" I' I " I ’" ' I'' Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

23719.D NP091101.M Tue Oct 16 15:14:26 2001 . Page 3

NYC-WTC_000089213

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NYC-WTC_000089213Source: NYC Law Department, mirrored locally

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