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GC/MS analysis results for sample AD23123, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23123 conducted on October 5, 2001, identifying unknown compounds.

NYC-WTC_000087942–000087952

Folder label: “GC/MS Scan 9/21/01

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Scanned page image, NYC-WTC_000087950
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT04 01\22974.D Vial: 7 Acq On 4 Oct 2001 9:24 pm Operator; 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 6.48 0.68 ug/1 104426 1,4-Dichlorobenzene-d4 11.78 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexyione 100 C6H12O 000591-78-6 91 2 2-Hex/none, 4-hydroxy-5-methyl-3-pr 172 C10H20O2 061141-74-0 78 3 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 78 4 Oxi3qfine, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 59 Abundance Scan 157 (6.484 min): 22974.D (-) m/z 42.95 100.00% 43

58 5000

_62P__§:40_a60_6;8g^_ I . ....... . , , , .l|l|l T-p-rr- I m/z 58.05 53.35% 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63384: 2-Hexanone 43

5000 58 6.20 6.40 6.60 6.80

Abundance ux20 29

30

4)3 50 60 70 80 90 100 #15807: 2-Hexanone, 4-hydraxy-5-methyl-3-propyl- 110 120 130 140 "m/z SYTOO 15.15%

6.20 6.40 6.60 6.80 5000 “mTz 41.00 14.81% 58 27 72

■n/z-> 20 ' ' I ' ' ' L 30 50 60 J....... 85....... 100................................. 70 80 90 100 110 120 130 140 Abundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- 43 _6;20__a40__a6g_a80__ m/z 100.05 10.56% 58 '.......... 553 29

' I' ' ' ‘ I ' ' '' 11 ,1 ' I''' 140 [\ Tl/Z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.20 6.40 6.60 6.80

22974.n MPnqi1m m T7t-t Orit- nq ii.nn.OT onm NYC-WTC_000087950

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NYC-WTC_000087950Source: NYC Law Department, mirrored locally

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