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GC/MS analysis results for sample AD22918, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22918 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087599–000087622

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0201\22918.D Vial: 8 Acq On : 2 Oct 2001 8:57 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params-. LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NPO91101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Tetratriacontane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 34.64 1.30 ug/1 178371 Chrysene-dl2 33.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetratriacontane 479 C34H70 014167-59-0 87 2 Octadecane 254 C18H38 000593-45-3 87 3 Tetracosane 338 C24H50 000646-31-1 87 4 Pentacosane 352 C25H52 000629-99-2 87 Abundance Scan 3224 (34.636 min): 22918.D (-) m7z 57700 100.00% 57 I 5000 85

221 34.40 34.60 34.80 35.00 169 197 1 ''"P" ' I" '' I " " I' m/z TITOO 64.49% m/z-> 40 60 80 100120140 160180 200 220 240 260 280 300 320 340 360 380 400 A Abundance #58265: Tetratriacontane 57

550 85 T 34.40 34.60 34.80 35.00 Wz 43.00 62.16% II I 113

Ti/z-> JlJUUr , 141 169 .............................. 40 60 80 100 120140160180 200 220 240 260 280 300 320 340 360 380 400 311 P '■•‘T 367 410 I""I'” •pH.I

Sundance #71561: Octadecane 5(7

T A 34.40 34.60 34.80 35.00 85 5000 m/z 85705 43.89%

224 254 I"'*I""I‘ ‘ I'' " I' prrrprrnTTrrrpTTTjrrT^^ n/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #73543: Tetracosane -p, ... 1 , 7', ,, 1 ,,,,,, , 57 34.40 34.60 34.80 35.00 m/z 55700 21.94%

5000 85

I I 113 155 183 294 338 .... . ■n/z-> 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 360 380 400 34.40 34.60 34.80 35.00

22918.D NP091101.M Thu Oct 04 09:43:01 2001 Page 12

NYC-WTC_000087617

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NYC-WTC_000087617Source: NYC Law Department, mirrored locally

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