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GC/MS analysis results for sample AD22917, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22917 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087586–000087598

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0201\22917.D Vial: 7 Acq On : 2 Oct 2001 7:59 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2,3-Diethylpyrazine Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 15.40 27.37 ug/1 3096390 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,3-Diethylp^azine 136 C8H12N2 015707-24-1 64 £-2. Naphthalene7^8- 136 C10D8 001146-65-2 52 3 6H-Purin-6/one, 1,7-dihydro- 136 C5H4N4O 000068-94-0 9 4 2-Hydro:2^ 5-methylbenzaldehyde 136 C8H8O2 000613-84-3 9 'Abundance Scan 1129 (15,402 min): 22917,0 (-) m/z 136.05 100.00% 156

5000

J y 15,00 15,20 15,40 15,60 15,80 1 m/z 137.05 10.55% TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6509: 2,3-Diethylpyrazine 1?1 136

5000- 15.00 15.20 15,40 15.60 15,80 80 107 m/z 134.00 8.59% 52 ,, hi I,,,,..... • I « > I • I I b I I I I I I I I . I I I 'I'Jif-'ir....... I Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 ^bundance #6596: Naphthalene-d8- 136 V ■r 15,00 15,20 15,40 15,60 15,80 m/z54700 7.64%

66 k-p-r-T-T-p-T-rn-r^^^n-p-|-r.-rT-nt-rT^74t4-H-?^^ 76 82 90 i i I Tife-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #65642: 6H-Purin-6-one, 1,7-dihydro- I ' ' ' ' I ' ' 136 15,00 15,20 15,40 15,60 15,80 m/z68.00 7.50%

5000- 54

27 38 ...........1 68........ ............................. 109..................... , , ■p-r-r-r-p-r V nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 15,00 15,20 15,40 15,60 15,80

22917.D NP091101.M Wed Oct 03 11:08:02 2001 Page 4

NYC-WTC_000087597

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