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GC/MS analysis results for sample AD22753, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22753 conducted on October 11, 2001, noting other unknown compounds.

NYC-WTC_000087390–000087402

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087399
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\SEP2801\22753.D Vial: 18 Acq On 29 Sep 2001 5:06 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 1

R.T. Area Relative to ISTD R.T.

6.48 0.63 ug/1 75260 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hex^one 100 C6H12O 000591-78-6 91 2 Meth^ Isobutyl Ketone 100 C6H12O 000108-10-1 64 3 Oxirane, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 50 4 2-]^xanone, 4-hydroxy-3-propyl-158 C9H18O2 062338-17-4 39 ^bundanoj Scan 157 (6.479 min): 22753.D (-) m/z 42.95 100.00% 413

58

I 5000

6.20 AJ 6.40 6.60 6.80 I m/z 58.0,5 59.34% im/z--> 20 25 .30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 S^bundance #1556: 2-Hexanone 413

58 5000 6.20 6.40 6.60 6.80 m/z 41.05 15.98% 27 39 71 85 100 4^ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63350: Methyl Isobutyl Ketone 43

6.20 6.40 6.60 6.80 5000 m/z 57„.00 14.37% 58 I 85 100 27 39 : I l! 67 Tn/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1530: Oxirane. 2-methyl-2-(1-methylethyl)- 413 6.20 6.40 6.60 6.80 58 m/ Z 84.95 9.95%

m/z~> 5000

30 66 •I I " " I *-'• 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 71 85 100 ..AJ 6.20 6.40 k Ai 6.60 6.80

22753.D NP091101.M Fri Oct 05 16:08:42 2001 Page 2

NYC-WTC_000087399

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NYC-WTC_000087399Source: NYC Law Department, mirrored locally

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