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GC/MS analysis results for sample AD22582, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22582 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087250–000087273

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087260
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2801\22582.D Vial: 10 Acq On : 28 Sep 2001 9:15 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 6.74 0.44 ug/1 55422 1,4-Dichlorobenzene-d4 11.79 Hit# of Tentative ID MW MolFoirm CAS# Qual 1 2-He^nol 102 C6H14O 000626-93-7 83 2 2-P^tanol, 4-methyl- 102 C6H140 000108-11-2 74 3 2-^ptanol, (S) - 116 C7H16O 006033-23-4 40 4 2/Butanol 74 C4H10O 000078-92-2 39 Abundance Scan 185 (6.742 min): 22582.D (-) m/z 44.95 100.00% 40

5000

69 60 33 87 6.40 6.60 6.80 7.00 I" " I'' " I" " I " " I ....... -I I" " I" " I"' h' " I' I" " I' r "' I m/ z 69.00 19.09% Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63584; 2-Hexanol 45

5000 6.40 6.60 6.80 7.00 69 Wz 41.05 14.24% 19 27 . 56 I 87 l^TTTTn+rlVTTTTTTTTTT+ll- lTTTri,ll|-HT7|,llipill|llll|

n/z-> 10 15 20 25 30 35.40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63545; 2-Pentanol, 4-methyl- 40 6.40 6.60 6.80 7.00 5000 m/ z 43.95 11.84%

69 27 39 , 57 87 lrrTiiiii|llin n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #3355:2-Heptanol, (S)- 4 6.40 6.60 6.80 7.00 m/z 43.00 10.32%

5000

55 2/ 39 I I 70 83 101 7TTTTp-rTTyTTTTpr4TTyTrrTJTTTtyrm- . I I I I ■ I . I p 1 I I I I ■■ I I ■ I ■ I I I I I I I I ■ I I I I I 1 < I I I I I I I I I I I I ■ I I I . I I I I I I I I I ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' tn/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.40 6.60' 6.80 7.00

22582.D NP091101.M Wed Oct 03 12:09:02 2001 Page 3

NYC-WTC_000087260

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NYC-WTC_000087260Source: NYC Law Department, mirrored locally

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