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GC/MS analysis report for sample AD22544, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22544 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086913–000086932

Folder label: “508 Scan 9/17/01 9/26/01

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Scanned page image, NYC-WTC_000086922
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2501\22544.D Vial: 10 Acq On : 25 Sep 2001 11:15 pm Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

6.50 0.49 ug/1 58595 1,4-Dichlorobenzene-d4 11.79 Hit# of Tentative ID MW MolForm CAS# Qual 1 2-I^anone 100 C6H12O 000591-78-6 90 2 2-jrfexanone, 4-hydroxy-5-methyl-3-pr 172 C10H20O2: 061141-74-0 74 3 ^Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 72 4/2-Hexanone, 4-methyl- 114 C7H14O 000105-42-0 39 fndance Scan 159 (6.497 min); 22544.D (-) m7z 42795 100.00% 43

58 553

85 100 _a20__a40_a60__6;80^_ 71 ..... , I I TT-p-T-T-I'l I I I I I I I I I I I 1 I 1 I I m/z 58.05 50.92% Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1556: 2-Hexanone 43

58 ...,,.,.7.77^7^,-,,,. 5000 6.20 6.40 6.60 6.80 “m/z 41.00 13.42% 27 I nZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #15807: 2-Hexanone, 4-hydroxy-5-methyl-3-propyl- 4)3

6.20 6.40 6,60 6.80 5000 m/z 100.05 11747% 58 27 72 I I.. 85.. 100............. nZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- A A 43 _6,20__6;40_a60__a80__ m/z 57.05 11.07% 29 58 I 5000

' I " '*'‘1 " " 11' ,1, ' I ' ' ' ' I ' 71 85 100 140 •n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.20 6.40 6.60 6.80

22544.D NP091101.M Mon Oct 01 12:58:59 2001 Page 1

NYC-WTC_000086922

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NYC-WTC_000086922Source: NYC Law Department, mirrored locally

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