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GCMS analysis results for sample AD24395, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of environmental sample AD24395 with detection of unknown compounds.

NYC-WTC_000068266–000068280

Folder label: “508 GCMS Scan X 10/11/01 An 11/2/01

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Scanned page image, NYC-WTC_000068275
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24395.D Vial: 12 Acq On : 2 Nov 2001 1:46 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.41 0.67 ug/1 97328 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexa: .e 100 C6H12O 000591-78-6 91 2 2-He: tone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 74 3 2- :anone, 4-hydroxy-5-methyl-3-pr 172 C10H20O2 061141-74-0 59 4 rane, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 50 ance Scan 149 (6.414 min); 24395.D (-) Tm/z 42.95 100.00% 43

58 5000 ........................... 71 85 ITO 6.00 “ 6JO " 6.^ " 6.M RM 'l ' ' ' ' 1'’' ' ' I ' ' ‘ ' I ' '' ' I''' ' I ' ' ' ' I ‘ ‘ I ‘ ‘ ' 1 ' m/z 58.05 53.06% nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 ^bundance #1556; 2-Hexanone 43

58 5000 6.00 6.20 6.40 6.60 6.80 m/z 41.00 18.20% 27 71 85 100 I I .. I ' I ' * ' ' I ’ ' ' ' H I '' ‘ ' I '' ' ' I ' •nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968; 2-Hexanone. 4-hydroxy-3-propyl- 43

58 6.00 6.20 6.40 6.60 6.80 5000 29 m/z 57.00 13.99% 1 I‘I'"‘''I' -t+ J. 71 I w ........ 140 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 —J Abundance #15807; 2-Hexanone, 4-hydroxy-5-methyl-3-propyl- 4)3 6.00 6.20 6.40 6.60 6.80 m/z 84.95 9734% 5000 58 27

nZz-> J, 20 30 ' ‘ p ' ' ' I ' 40 50 1 60 70 72

80 90 100 110 120 IM W 4 6.60 6.80

24395.D NP103001.M Wed Nov 07 14:31:14 2001 Page 1

NYC-WTC_000068275

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NYC-WTC_000068275Source: NYC Law Department, mirrored locally

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