VOC analysis results, sample AE12279, May 2002

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Data File : C:\HPCHEM\l\DATA\02MAY23\12280.D Vial: 5 Acq On : 23 May 2002 8:34 pm Operator: 201-wb Sample : nys Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title VOCs BY EPA METHOD 524 Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 22.68 0.09 ug/L 78646 CHLOROBENZENE-D5 21.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 74 2 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 3 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 4 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 5 Abundance Scan 1099 (22.679 min): 12280.D (-) m/z 281.25 100.00% 2( 11

Wilil

73 133 191 207 265 22.40 22.60 22.80 23.00 44 I I I I m/z 282.25 29.54% tt/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72646: Cycloletrasiloxane, octamethyl- 21 11

5000 22.40 22.60 22.80 23.00 m/z 283.25 18.71% 265 73 133 45 59 I 177 yy 235 JL m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624:3,6-Bis(N-dimethylamino)-9-ethylcarbazole 2( 11

22.40 22.60 22.80 23.00 5000 m/z 133.05 10.19% 266 A 141 o-5r250 2082222dD I I ■ I'' l'’' ''I I... . TT/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 2$1 ..... 1,1...... 22.40 22.60 22.80 23.00 m/z 73.05 8.74% f\ 5000

....................... TTYTTTn-TTTT-TJ-rrTT-yr^ T T I TT/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

12280.D HP051702.M Fri May 24 15:02:47 2002 Page 3

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