VOC analysis results, sample AE12279, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\l\DATA\02MAY23\0523C10B.D Vial: 2 Acq On : 24 May 2002 3:47 am Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: GAS6.P Quant Time: May 31 12:03.2002 Quant Results File: HP051702.RES Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu May 23 09:09:18 2002 Response via : Initial Calibration DataAcq Meth : HP051702

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.12 114 1344613 5.00 ug/L 0.09 24) CHLOROBENZENE-D5 21.78 117 1313443 5.00 ug/L 0.07 52) 1,4-DICHLOROBENZENE-D4 26.95 152 684980 5.00 ug/L 0.07

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.35 65 694782 5.29 ug/L 0.09 Spiked Amount 5.000 Recovery = 105.80% 3) 4-BROMOFLUOROBENZENE 24.36 174 559485 5.90 ug/L 0.07 Spiked Amount 5.000 Recovery = 118.00% 25) TOLUENE-D8 18.47 98 1708891 4.76 ug/L 0.07 Spiked Amount 5.000 Recovery = 95.20% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.85 85 501835 9.69 ug/L 99 5) CHLOROMETHANE 5.37 50 954998 11.86 ug/L 98 6) VINYL CHLORIDE 5.58 62 409324 10.04 ug/L 99 7) BROMOMETHANE 6.57 94 179493 8.63 ug/L 100 8) CHLOROETHANE 6.72 64 458874 11.42 ug/L 97 9) TRICHLOROFLUOROMETHANE 7.28 101 726340 9.65 ug/L 99 11) l,l,2-Trichloro-l,2,2-trif 8.17 101 400296 9.31 ug/L 100 12) ACETONE 8.26 43 424452 35.64 ug/L 99 13) 1,1-DICHLOROETHENE 8.62 61 1114043 11.53 ug/L 99 14) METHYLENE CHLORIDE 9.62 49 1198708 13.60 ug/L 96 15) METHYL TERT BUTYL ETHER 9.93 73 817135 11.96 ug/L 97 16) TRANS-1,2-DICHLOROETHENE 10.28 61 1297630 13.24 ug/L 90 17) 1,1-DICHLOROETHANE 11.17 63 1426859 13.45 ug/L 99 18) 2-BUTANONE (MEK) 12.00 43 518151 57.94 ug/L 91 19) 2,2 -DICHLOROPROP7\NE 12.40 . 77 826907 9.61 ug/L 100 20) CIS-1,2-DICHLOROETHENE 12.48 96 736143 12.78 ug/L 92 21) CHLOROFORM 12.82 83 1433767 12.63 ug/L 100 22) BROMOCHLOROMETHANE 13.20 49 668271 14.96 ug/L 84 23) 1,2-DICHLOROETHANE 14.54 62 1168036 13.76 ug/L 98 26) 1,1,1-TRICHLOROETHANE 13.72 97 1062035 9.94 ug/L 99 27) 1,1-DICHLOROPROPENE 14.05 75 1100980 11.07 ug/L 99 28) CARBON TETRACHLORIDE 14.30 117 875967 9.97 ug/L 98 29) BENZENE 14.64 78 2570439 11.97 ug/L 99 30) TRICHLOROETHENE 15.92 95 801795 11.20 ug/L 95 31) 1,2-DICHLOROPROPANE 16.28 63 738909 12.75 ug/L 96 3 2) DIBROMOMETHANE 16.96 174 330109 11.75 ug/L 95 33) BROMODICHLOROMETHANE 16.79 83 972095 11.53 ug/L 99 34) 2-CHLOROETHYL VINYL ETHER 17.28 63 199745 17.88 ug/L 96 35) METHYL ISO-BUTYL KETONE 17.35 58 407253 56.09 ug/L 84 36) CIS-1,3-DICHLOROPROPENE 17.89 75 964393 11.82 ug/L 98 37) TOLUENE 18.64 91 2659762 12.14 ug/L 100 38) TRANS-1,3-DICHLOROPROPENE 18.92 75 708099 10.44 ug/L 97 39) 1,1,2-TRICHLOROETHANE 19.31 97 427724 12.67 ug/L 97 40) TETRACHLOROETHENE 20.09 166 739492 11.45 ug/L 97 41) 1,3-DICHLOROPROPANE 19.84 76 853501 13.02 ug/L 97 42) DIBROMOCHLOROMETHANE 20.53 129 497820 12.19 ug/L 96 43) 1,2-DIBROMOETHANE 20.98 107 418150 11.90 ug/L 99 44) CHLOROBENZENE 21.86 112 1651109 12.44 ug/L 97 45) 1,1,1,2-TETRACHLOROETHANE 21.91 131 608399 11.87 ug/L 97 46) 2-HEXANONE 19.21 43 812383 58.47 ug/L 98 ■47) ETHYLBENZENE 21.90 91 3135058 12.14 ug/L 99 (#) = qualifier out of range (m) = manual integration 0523C10B.D HP051702.M Fri May 31 12:03:14 2002 Page 1

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