VOC analysis results, sample AE11905, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File C:\HPCHEM\l\DATA\02MAY22\0522C10B.D Vial 3 Acq On 22 May 2002 10:04 pm Operator 201-wb Sample cal 10 Inst GC/MS Ins Mise Multiplr 1.00 MS Integration Params: GAS6.P Quant Time: Jun 3 14:23 2002 Quant Results File: HP051702.RES

Quant Method C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title VOCs BY EPA METHOD 524 Last Update Fri May 31 11:43:42 2002 Response via Initial Calibration DataAcq Meth HP052102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.07 114 1163302 5.00 ug/L 0.03 24) CHLOROBENZENE-D5 21.73 117 1105681 5.00 ug/L 0.02 52) 1,4-DICHLOROBENZENE-D4 26.90 152 560544 5.00 ug/L 0.02

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.30 65 563412 4.96 ug/L 0.03 ■ Spiked Amount 5.000 Recovery = 99.20% 3) 4-BROMOFLUOROBENZENE 24.31 174 449297 5.48 ug/L 0.02 Spiked Amount 5.000 Recovery = 109.60% 25) TOLUENE-D8 18.42 98 1457284 4.83 ug/L 0.02 Spiked Amount 5.000 Recovery = 96.60% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.83 85 295858 7.09 ug/L 100 5) CHLOROMETHANE 5.34 50 641964 9.22 ug/L 96 6) VINYL CHLORIDE 5.57 62 308348 8.65 ug/L 99 7) BROMOMETHANE 6.54 94 164277 9.06 ug/L 99 8) CHLOROETHANE 6.69 64 342286 9.84 ug/L 98 9) TRICHLOROFLUOROMETHANE 7.25 101 572001 8.79 ug/L 97 11) l,l,2-Trichloro-l,2,2-trif 8.14 101 348145 9.36 ug/L 95 12) ACETONE 8.22 43 272138 26.42 ug/L 99 13) 1,1-DICHLOROETHENE 8.57 61 860684 10.29 ug/L 99 14) METHYLENE CHLORIDE 9.57 49 824477 10.81 ug/L 97 15) METHYL TERT BUTYL ETHER 9.88 73 585636 9.91 ug/L 98 16) TRANS-1,2-DICHLOROETHENE 10.23 61 960912 11.33 ug/L 91 17) 1,1-DICHLOROETHANE 11.14 63 1039085 11.32 ug/L 100 18) 2-BUTANONE (MEK) 11.95 43 321282 41.53 ug/L 94 19) 2,2-DICHLOROPROPANE 12.34 77 718527 9.65 ug/L 98 20) CIS-1,2-DICHLORbETHENE 12.45 96 568676 11.42 ug/L 99 21) CHLOROFORM 12.77 83 1079907 10.99 ug/L 100 22) BROMOCHLOROMETHANE 13.16 49 452514 11.71 ug/L 97 23) 1,2-DICHLOROETHANE 14.51 62 821166 11.18 ug/L 99 26) 1,1,1-TRICHLOROETHANE 13.67 97 838188 9.32 ug/L 100 27) 1,1-DICHLOROPROPENE 14.00 75 833227 9.95 ug/L 100 28) CARBON TETRACHLORIDE 14.25 117 693737 9.38 ug/L 99 29) BENZENE 14.59 78 1907276 10.55 ug/L 100 30) TRICHLOROETHENE 15.87 95 612642 10.17 ug/L' 95 31) 1,2-DICHLOROPROPANE 16.23 63 524188 10.75 ug/L 98 32) DIBROMOMETHANE 16.91 174 244442 10.-34 ug/L 90 3 3) BROMODICHLOROMETHANE 16.74 83 724047 10.20 ug/L 96 34) 2-CHLOROETHYL VINYL ETHER 17.23 63 142768 15.18 ug/L 98 35) METHYL ISO-BUTYL KETONE 17.30 58 268811 43.98 ug/L 94 36) CIS-1,3-DICHLOROPROPENE 17.84 75 715110 10.41 ug/L 99 37) TOLUENE 18.59 91 1969871 10.68 ug/L 98 38) TRANS-1,3-DICHLOROPROPENE 18.87 75 511717 8.92 ug/L 99 39) 1,1,2-TRICHLOROETHANE 19.26 97 304435 10.71 ug/L 99 40) TETRACHLOROETHENE 20.04 166 564527 10.38 ug/L 95 41) 1,3-DICHLOROPROPANE 19.78 76 603848 10.94 ug/L 96 42) DIBROMOCHLOROMETHANE 20.48 129 368815 10.73 ug/L 95 43) 1,2-DIBROMOETHANE 20.93 107 307436 10.39 ug/L 99 44) CHLOROBENZENE 21.81 112 1235368 11.05 ug/L 98 45) 1,1,1,2-TETRACHLOROETHANE 21.86 131 455757 10.56 ug/L 96 46) 2-HEXANONE 19.15 43 508514 43.47 ug/L 99 47) ETHYLBENZENE 21.84 91 2348504 10.81 ug/L 97

(#) = qualifier out of range (m) = manual integration 0522C10B.D HP051702.M Mon Jun 03 14:24:00 2002 Page 1

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